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The glycosylation of human synovial lubricin: implications for its role in inflammation

GlyToucan Accession Number: G18132YR

Peak	Intensity
253.34	842.0
407.21	1089.0
Annotations: YZ ZY
473.87	789.0
491.21	1062.0
569.21	4820.0
Annotations: Z Z
569.83	72.0
588.37	533.0
615.86	438.0
620.86	968.0
730.48	420.0

There are 16 similar spectra:

Id	Structure	Score
3659		0.88
24		0.88
2675		0.88
3051		0.87
187		0.87
2638		0.87
100		0.87
2777		0.86
3052		0.86
279		0.85
330		0.84
42		0.80
458		0.78
2778		0.76
25		0.76
188		0.76

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass 748.29
(Calculated Monoisotopic)

Reducing End Reduced

Persubstitution Underivatised

Biological Context

Taxonomy - Homo Sapiens

Tissue - Synovial Fluid

Glycoprotein - Proteoglycan 4

HPLC

Column Custom made Hypercarb

Method

60 gradient with 10 run rate
10mM Ammonium Bicarbonate
80% Acetonitrile in 10mM Ammonium Bicarbonate

Mass Spec

Thermo Fisher XP ESI

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