Versatile Separation and Analysis of Heparan Sulfate Oligosaccharides using Graphitised Carbon Liquid Chromatography and Electrospray Mass Spectrometry
| Peak | Intensity |
|---|---|
| 236.6 | 186.0 |
| 259.8 | 144.0 |
|
Annotations: BZ |
|
| 300.7 | 451.0 |
| 318.1 | 168.0 |
|
Annotations: Y |
|
| 357.9 | 218.0 |
|
Annotations: Y |
|
| 396.0 | 225.0 |
|
Annotations: CY |
|
| 416.0 | 428.0 |
|
Annotations: C |
|
| 437.0 | 165.0 |
|
Annotations: Z |
|
| 437.9 | 135.0 |
|
Annotations: Z |
|
| 473.7 | 159.0 |
| 476.1 | 239.0 |
|
Annotations: B |
|
| 486.9 | 172.0 |
|
Annotations: Y |
|
| 496.0 | 1220.0 |
|
Annotations: Z |
|
| 496.9 | 255.0 |
| 517.0 | 139.0 |
| 526.6 | 2130.0 |
|
Annotations: Y |
|
| 527.6 | 298.0 |
| 549.3 | 162.0 |
| 556.0 | 211.0 |
| 557.1 | 956.0 |
|
Annotations: Y |
|
| 562.9 | 483.0 |
| 564.7 | 248.0 |
| 565.7 | 5417.0 |
| 566.0 | 4876.0 |
| 567.0 | 927.0 |
|
Annotations: Y |
|
| 574.1 | 1071.0 |
|
Annotations: B |
|
| 575.1 | 567.0 |
| 584.5 | 277.0 |
| 587.6 | 352.0 |
| 588.6 | 128.0 |
| 592.0 | 131.0 |
|
Annotations: C |
|
| 596.6 | 5430.0 |
| 603.7 | 656.0 |
| 605.6 | 121840.0 |
| 608.7 | 319.0 |
| 613.3 | 243.0 |
| 627.1 | 210.0 |
| 627.7 | 432.0 |
| 631.5 | 789.0 |
| 635.0 | 1372.0 |
| 636.0 | 317.0 |
| 656.5 | 175.0 |
| 714.7 | 22.0 |
| 717.2 | 42.0 |
|
Annotations: Y |
|
| 735.2 | 25.0 |
| 736.1 | 116.0 |
| 737.7 | 48.0 |
| 752.8 | 215.0 |
| 753.2 | 303.0 |
| 777.3 | 133.0 |
|
Annotations: B |
|
| 790.9 | 31.0 |
| 795.2 | 60.0 |
|
Annotations: C |
|
| 796.5 | 82.0 |
| 797.3 | 78.0 |
| 813.2 | 148.0 |
|
Annotations: Y |
|
| 813.9 | 55.0 |
| 816.4 | 3.0 |
| 819.6 | 33.0 |
| 824.2 | 75.0 |
| 830.8 | 28.0 |
| 832.2 | 161.0 |
| 850.3 | 23.0 |
| 853.2 | 47.0 |
| 854.4 | 66.0 |
| 892.1 | 8.0 |
| 896.1 | 34.0 |
| 910.4 | 71.0 |
| 911.3 | 355.0 |
| 912.3 | 215.0 |
| 928.2 | 73.0 |
| 953.4 | 29.0 |
|
Annotations: B |
|
| 974.9 | 15.0 |
| 1003.3 | 35.0 |
| 1034.5 | 116.0 |
| 1035.5 | 96.0 |
| 1038.0 | 65.0 |
| 1047.1 | 147.0 |
| 1054.4 | 38.0 |
|
Annotations: Y |
|
| 1066.4 | 41.0 |
| 1070.3 | 13.0 |
| 1077.3 | 26.0 |
| 1096.3 | 56.0 |
| 1097.5 | 78.0 |
| 1105.1 | 86.0 |
| 1113.4 | 40.0 |
| 1114.3 | 565.0 |
| 1115.3 | 334.0 |
| 1116.5 | 144.0 |
|
Annotations: Z |
|
| 1117.1 | 86.0 |
| 1117.7 | 30.0 |
| 1150.2 | 139.0 |
| 1154.5 | 67.0 |
| 1190.7 | 84.0 |
| 1193.0 | 32.0 |
| 1194.4 | 490.0 |
| 1195.4 | 91.0 |
| 1196.3 | 26.0 |
| 1197.2 | 14.0 |