Versatile Separation and Analysis of Heparan Sulfate Oligosaccharides using Graphitised Carbon Liquid Chromatography and Electrospray Mass Spectrometry
| Peak | Intensity |
|---|---|
| 264.8 | 120.0 |
|
Annotations: CY |
|
| 319.8 | 256.0 |
| 358.0 | 14.0 |
| 377.9 | 19.0 |
|
Annotations: Z |
|
| 395.9 | 55.0 |
|
Annotations: Y |
|
| 397.0 | 15.0 |
|
Annotations: Z |
|
| 399.0 | 267.0 |
| 411.7 | 16.0 |
| 414.9 | 59.0 |
|
Annotations: B |
|
| 416.0 | 248.0 |
|
Annotations: C |
|
| 444.1 | 34.0 |
| 446.8 | 204.0 |
|
Annotations: Y |
|
| 455.5 | 202.0 |
|
Annotations: B |
|
| 456.8 | 16.0 |
| 471.3 | 32.0 |
| 476.0 | 477.0 |
| 476.9 | 128.0 |
| 477.9 | 121.0 |
|
Annotations: Z |
|
| 481.0 | 28.0 |
| 482.9 | 83.0 |
| 483.4 | 321.0 |
| 486.5 | 16.0 |
|
Annotations: Y |
|
| 489.0 | 58.0 |
| 494.0 | 45.0 |
|
Annotations: B |
|
| 495.0 | 1293.0 |
|
Annotations: B |
|
| 496.0 | 1035.0 |
|
Annotations: C |
|
| 506.7 | 61.0 |
| 508.1 | 78.0 |
| 512.1 | 13.0 |
|
Annotations: C |
|
| 515.2 | 252.0 |
|
Annotations: CY |
|
| 516.4 | 134.0 |
| 526.5 | 667.0 |
|
Annotations: Y |
|
| 527.5 | 53.0 |
| 528.4 | 44.0 |
| 534.2 | 151.0 |
| 535.0 | 132.0 |
|
Annotations: B |
|
| 539.9 | 55.0 |
| 540.5 | 58.0 |
| 541.1 | 184.0 |
| 547.5 | 35.0 |
| 555.2 | 79.0 |
| 555.8 | 94.0 |
| 556.5 | 399.0 |
| 557.7 | 211.0 |
| 558.9 | 44.0 |
|
Annotations: BZ |
|
| 563.1 | 222.0 |
| 564.0 | 123.0 |
| 564.7 | 143.0 |
| 565.6 | 3651.0 |
| 566.0 | 3181.0 |
| 568.6 | 6.0 |
| 569.7 | 23.0 |
| 572.7 | 199.0 |
| 576.1 | 196.0 |
| 577.0 | 54.0 |
|
Annotations: BY |
|
| 584.7 | 25.0 |
| 587.6 | 403.0 |
| 594.7 | 150.0 |
|
Annotations: CY |
|
| 595.7 | 60.0 |
| 596.6 | 1436.0 |
| 597.0 | 709.0 |
| 603.1 | 135.0 |
| 605.6 | 69393.0 |
| 608.5 | 53.0 |
| 609.7 | 28.0 |
|
Annotations: CY |
|
| 610.7 | 41.0 |
| 616.4 | 17.0 |
| 621.1 | 58.0 |
| 621.9 | 15.0 |
| 622.7 | 168.0 |
| 626.9 | 177.0 |
| 636.2 | 148.0 |
| 636.5 | 171.0 |
| 637.1 | 159.0 |
|
Annotations: Y |
|
| 638.1 | 319.0 |
| 639.1 | 12.0 |
|
Annotations: BZ |
|
| 644.7 | 49.0 |
| 654.9 | 47.0 |
|
Annotations: B |
|
| 673.4 | 106.0 |
|
Annotations: C |
|
| 694.0 | 6.0 |
| 699.2 | 73.0 |
| 717.1 | 51.0 |
| 734.1 | 53.0 |
| 735.1 | 141.0 |
|
Annotations: B |
|
| 736.5 | 31.0 |
| 740.2 | 60.0 |
| 741.2 | 43.0 |
| 752.3 | 62.0 |
| 753.2 | 65.0 |
|
Annotations: C |
|
| 753.9 | 28.0 |
| 756.4 | 97.0 |
| 771.4 | 150.0 |
|
Annotations: CY |
|
| 801.6 | 81.0 |
| 813.1 | 40.0 |
|
Annotations: Y |
|
| 835.9 | 55.0 |
| 876.5 | 25.0 |
|
Annotations: Z |
|
| 892.1 | 15.0 |
| 894.1 | 93.0 |
|
Annotations: Y |
|
| 899.0 | 80.0 |
| 909.4 | 24.0 |
| 911.2 | 496.0 |
|
Annotations: B |
|
| 912.4 | 230.0 |
| 914.4 | 212.0 |
| 915.0 | 200.0 |
| 930.1 | 8.0 |
| 976.0 | 18.0 |
| 984.3 | 74.0 |
| 984.6 | 34.0 |
| 990.2 | 19.0 |
| 993.1 | 41.0 |
| 1016.5 | 57.0 |
| 1034.6 | 67.0 |
| 1052.3 | 11.0 |
| 1060.4 | 28.0 |
| 1070.5 | 21.0 |
| 1094.2 | 24.0 |
| 1095.3 | 41.0 |
| 1096.4 | 260.0 |
| 1114.4 | 495.0 |
| 1115.3 | 268.0 |
| 1116.5 | 149.0 |
| 1117.7 | 36.0 |
| 1176.4 | 58.0 |
| 1177.5 | 43.0 |
| 1192.1 | 16.0 |
| 1194.1 | 17.0 |
| 1194.8 | 27.0 |
| 1195.6 | 9.0 |
| 1196.2 | 111.0 |