Versatile Separation and Analysis of Heparan Sulfate Oligosaccharides using Graphitised Carbon Liquid Chromatography and Electrospray Mass Spectrometry

PubMed Entry

Peak Intensity
182.7 58.0
284.7 38.0
298.9 397.0
300.8 168.0
357.8 84.0
377.4 136.0
378.0 218.0

Annotations:

BY CZ BY CZ
379.2 52.0
394.0 96.0
398.0 167.0

Annotations:

B
399.0 131.0
405.5 173.0
416.0 226.0

Annotations:

C Z
416.9 23.0
436.3 34.0

Annotations:

B
437.5 62.0

Annotations:

C Z
455.4 216.0
464.3 83.0
476.1 383.0

Annotations:

B
486.4 35.0

Annotations:

Y
487.1 121.0

Annotations:

Y
495.0 2554.0
496.0 1659.0

Annotations:

C
504.0 159.0
506.4 162.0
510.3 256.0
512.1 222.0

Annotations:

C
512.9 125.0
515.0 382.0
515.7 485.0

Annotations:

B
516.5 98.0

Annotations:

B
517.4 203.0

Annotations:

Z
518.1 166.0
519.1 53.0
525.0 33.0

Annotations:

C
525.5 270.0

Annotations:

C
526.5 2059.0

Annotations:

Y
528.2 382.0
531.1 178.0
532.1 33.0
532.9 47.0
537.9 5.0
539.5 113.0

Annotations:

Z
540.7 47.0
541.1 25.0
545.5 10.0
546.5 173.0
547.5 508.0
551.9 95.0
555.1 591.0
556.5 689.0
557.3 691.0

Annotations:

Y
558.0 143.0
563.5 347.0
564.0 273.0
565.6 11579.0
566.1 8358.0
568.6 11.0
569.9 73.0
570.1 53.0
572.9 671.0
574.9 683.0
576.5 431.0
578.4 78.0
581.5 42.0
582.4 268.0
584.6 35.0
585.7 125.0
586.7 68.0
587.6 720.0
588.0 784.0
596.6 4610.0
600.0 52.0
602.9 52.0
604.1 1740.0
605.6 161851.0
608.6 47.0
610.8 129.0
612.4 678.0
614.2 78.0
615.6 233.0
619.0 35.0

Annotations:

Z
622.5 26.0
627.1 67.0
635.9 459.0
637.2 1818.0

Annotations:

Y
639.3 71.0
652.9 141.0
655.7 26.0
657.9 24.0
675.1 86.0
713.0 88.0
714.0 20.0
715.3 37.0

Annotations:

C Z
717.9 66.0
735.3 291.0
737.0 21.0
753.3 53.0
754.5 203.0
756.3 209.0
794.5 62.0
795.3 42.0

Annotations:

C Z
796.4 100.0
814.1 32.0
816.2 83.0
817.2 22.0
818.8 79.0
823.0 73.0
824.1 78.0
832.3 46.0
834.1 153.0
835.2 119.0
877.1 28.0
911.2 732.0
912.4 320.0
914.4 61.0
929.2 299.0
934.3 42.0
936.1 93.0
937.3 66.0
956.2 402.0

Annotations:

Z
967.3 89.0
971.4 68.0

Annotations:

C
974.5 104.0

Annotations:

Y
975.5 14.0
978.0 46.0
985.5 30.0
990.3 51.0
1016.3 46.0
1034.5 51.0
1036.5 227.0

Annotations:

Z
1069.5 133.0
1070.4 80.0
1082.6 13.0
1096.7 45.0
1097.6 833.0
1109.3 87.0
1113.4 25.0
1114.4 757.0
1115.4 1273.0
1116.4 322.0
1158.1 44.0
1172.4 90.0
1178.9 57.0
1193.3 16.0
1194.2 83.0
1195.5 225.0
1196.2 360.0
1199.1 20.0

There are 3 similar spectra:

Id Structure Score

3099

1.00

3102

1.00

3101

1.00
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