Versatile Separation and Analysis of Heparan Sulfate Oligosaccharides using Graphitised Carbon Liquid Chromatography and Electrospray Mass Spectrometry
| Peak | Intensity |
|---|---|
| 182.7 | 58.0 |
| 284.7 | 38.0 |
| 298.9 | 397.0 |
| 300.8 | 168.0 |
| 357.8 | 84.0 |
| 377.4 | 136.0 |
| 378.0 | 218.0 |
|
Annotations: BY |
|
| 379.2 | 52.0 |
| 394.0 | 96.0 |
| 398.0 | 167.0 |
|
Annotations: B |
|
| 399.0 | 131.0 |
| 405.5 | 173.0 |
| 416.0 | 226.0 |
|
Annotations: C |
|
| 416.9 | 23.0 |
| 436.3 | 34.0 |
|
Annotations: B |
|
| 437.5 | 62.0 |
|
Annotations: C |
|
| 455.4 | 216.0 |
| 464.3 | 83.0 |
| 476.1 | 383.0 |
|
Annotations: B |
|
| 486.4 | 35.0 |
|
Annotations: Y |
|
| 487.1 | 121.0 |
|
Annotations: Y |
|
| 495.0 | 2554.0 |
| 496.0 | 1659.0 |
|
Annotations: C |
|
| 504.0 | 159.0 |
| 506.4 | 162.0 |
| 510.3 | 256.0 |
| 512.1 | 222.0 |
|
Annotations: C |
|
| 512.9 | 125.0 |
| 515.0 | 382.0 |
| 515.7 | 485.0 |
|
Annotations: B |
|
| 516.5 | 98.0 |
|
Annotations: B |
|
| 517.4 | 203.0 |
|
Annotations: Z |
|
| 518.1 | 166.0 |
| 519.1 | 53.0 |
| 525.0 | 33.0 |
|
Annotations: C |
|
| 525.5 | 270.0 |
|
Annotations: C |
|
| 526.5 | 2059.0 |
|
Annotations: Y |
|
| 528.2 | 382.0 |
| 531.1 | 178.0 |
| 532.1 | 33.0 |
| 532.9 | 47.0 |
| 537.9 | 5.0 |
| 539.5 | 113.0 |
|
Annotations: Z |
|
| 540.7 | 47.0 |
| 541.1 | 25.0 |
| 545.5 | 10.0 |
| 546.5 | 173.0 |
| 547.5 | 508.0 |
| 551.9 | 95.0 |
| 555.1 | 591.0 |
| 556.5 | 689.0 |
| 557.3 | 691.0 |
|
Annotations: Y |
|
| 558.0 | 143.0 |
| 563.5 | 347.0 |
| 564.0 | 273.0 |
| 565.6 | 11579.0 |
| 566.1 | 8358.0 |
| 568.6 | 11.0 |
| 569.9 | 73.0 |
| 570.1 | 53.0 |
| 572.9 | 671.0 |
| 574.9 | 683.0 |
| 576.5 | 431.0 |
| 578.4 | 78.0 |
| 581.5 | 42.0 |
| 582.4 | 268.0 |
| 584.6 | 35.0 |
| 585.7 | 125.0 |
| 586.7 | 68.0 |
| 587.6 | 720.0 |
| 588.0 | 784.0 |
| 596.6 | 4610.0 |
| 600.0 | 52.0 |
| 602.9 | 52.0 |
| 604.1 | 1740.0 |
| 605.6 | 161851.0 |
| 608.6 | 47.0 |
| 610.8 | 129.0 |
| 612.4 | 678.0 |
| 614.2 | 78.0 |
| 615.6 | 233.0 |
| 619.0 | 35.0 |
|
Annotations: Z |
|
| 622.5 | 26.0 |
| 627.1 | 67.0 |
| 635.9 | 459.0 |
| 637.2 | 1818.0 |
|
Annotations: Y |
|
| 639.3 | 71.0 |
| 652.9 | 141.0 |
| 655.7 | 26.0 |
| 657.9 | 24.0 |
| 675.1 | 86.0 |
| 713.0 | 88.0 |
| 714.0 | 20.0 |
| 715.3 | 37.0 |
|
Annotations: C |
|
| 717.9 | 66.0 |
| 735.3 | 291.0 |
| 737.0 | 21.0 |
| 753.3 | 53.0 |
| 754.5 | 203.0 |
| 756.3 | 209.0 |
| 794.5 | 62.0 |
| 795.3 | 42.0 |
|
Annotations: C |
|
| 796.4 | 100.0 |
| 814.1 | 32.0 |
| 816.2 | 83.0 |
| 817.2 | 22.0 |
| 818.8 | 79.0 |
| 823.0 | 73.0 |
| 824.1 | 78.0 |
| 832.3 | 46.0 |
| 834.1 | 153.0 |
| 835.2 | 119.0 |
| 877.1 | 28.0 |
| 911.2 | 732.0 |
| 912.4 | 320.0 |
| 914.4 | 61.0 |
| 929.2 | 299.0 |
| 934.3 | 42.0 |
| 936.1 | 93.0 |
| 937.3 | 66.0 |
| 956.2 | 402.0 |
|
Annotations: Z |
|
| 967.3 | 89.0 |
| 971.4 | 68.0 |
|
Annotations: C |
|
| 974.5 | 104.0 |
|
Annotations: Y |
|
| 975.5 | 14.0 |
| 978.0 | 46.0 |
| 985.5 | 30.0 |
| 990.3 | 51.0 |
| 1016.3 | 46.0 |
| 1034.5 | 51.0 |
| 1036.5 | 227.0 |
|
Annotations: Z |
|
| 1069.5 | 133.0 |
| 1070.4 | 80.0 |
| 1082.6 | 13.0 |
| 1096.7 | 45.0 |
| 1097.6 | 833.0 |
| 1109.3 | 87.0 |
| 1113.4 | 25.0 |
| 1114.4 | 757.0 |
| 1115.4 | 1273.0 |
| 1116.4 | 322.0 |
| 1158.1 | 44.0 |
| 1172.4 | 90.0 |
| 1178.9 | 57.0 |
| 1193.3 | 16.0 |
| 1194.2 | 83.0 |
| 1195.5 | 225.0 |
| 1196.2 | 360.0 |
| 1199.1 | 20.0 |