Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.

PubMed Entry

GlyToucan Accession Number: G78032US

Peak Intensity
311.8 3828.0
324.0 3798.0
324.7 6867.3

Annotations:

C
325.4 0.7

Annotations:

C
364.0 4252.7

Annotations:

B
364.8 3180.7
381.8 4074.3

Annotations:

C
389.2 36650.7

Annotations:

ZZ ZZ
389.9 212.3
407.1 16586.3

Annotations:

ZY YZ ZY YZ
407.9 1693.7
408.9 13414.7
409.9 4494.7
423.7 3183.0

Annotations:

^{0,4}A_{GalNAc} ^{2,4}A_{GalNAc}Y
424.3 3142.0

Annotations:

^{0,4}A_{GalNAc} ^{2,4}A_{GalNAc}Y
427.0 4065.7

Annotations:

^{0,2}A_{GlcNAc}
437.9 1113.0

Annotations:

^{3,5}A_{GalNAc} ^{1,4}A_{GlcNAc}
442.1 5287.0
443.0 2025.7
467.0 2128.7
467.8 2499.7
479.0 579.3
508.9 4211.0
510.2 5701.3

Annotations:

B
511.0 819.0
521.0 4352.7
521.6 1811.0
527.0 18770.7
528.1 7943.0

Annotations:

C
532.4 830.3
540.6 1469.3
545.3 2203.0
550.0 876.3
551.2 11565.7

Annotations:

ZZ
552.1 1570.0
560.4 5014.0
569.1 288524.0

Annotations:

Z
570.1 28126.7

Annotations:

^{2,4}A_{GalNAc}
574.1 1762.7
587.0 32187.0

Annotations:

Y
587.7 1.3

Annotations:

Y
592.1 18229.3

Annotations:

ZZ
592.9 2500.7
609.9 8836.7

Annotations:

ZY YZ
625.0 9785.3
645.9 1629.7
652.0 655.0
681.9 1356.7
691.3 2243.7
694.9 3458.3
712.4 6792.7
715.0 6613.0

Annotations:

Z
715.9 7634.7
724.2 1962.3

Annotations:

^{1,5}A_{GalNAc}Z
730.3 5932.3
733.3 3896.7

Annotations:

Y
753.8 366.7

Annotations:

ZZ
756.6 1087.3
772.2 135497.3

Annotations:

Z
773.1 28127.0
790.1 1005.0

Annotations:

Y
795.6 161.7
834.4 4400.3
837.3 6733.7
841.8 4617.0
857.9 1681.7
858.5 850.0
875.0 2384.0
876.2 3311.3
892.7 1060.3
894.2 6842.3
895.3 7636.7
898.1 1189.3
900.1 2860.3
901.2 6806.3
918.2 23376.7

Annotations:

Z
919.1 4487.3
930.1 2312.7
933.9 1229.3

Annotations:

Z
935.0 4082.0
936.3 17217.3

Annotations:

Y
937.2 2214.0
953.2 804.0
978.4 4123.7
978.9 1011.0

Annotations:

^{2,5}A_{GalNAc}
983.6 3322.3
996.4 3567.3
997.2 4200.7
1015.1 426.0
1038.1 37442.7
1039.3 15455.3
1054.6 1201.7
1056.2 60818.3
1057.1 6095.3
1137.2 1441.7
1212.2 557.0

There are 12 similar spectra:

Id Structure Score

2975

0.86

2797

0.82

3679

0.82

494

0.80

521

0.71

2977

0.68

3678

0.67

206

0.66

164

0.66

205

0.66

2973

0.66

475

0.57
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