Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.
GlyToucan Accession Number: G78032US
| Peak | Intensity |
|---|---|
| 311.8 | 3828.0 |
| 324.0 | 3798.0 |
| 324.7 | 6867.3 |
|
Annotations: C |
|
| 325.4 | 0.7 |
|
Annotations: C |
|
| 364.0 | 4252.7 |
|
Annotations: B |
|
| 364.8 | 3180.7 |
| 381.8 | 4074.3 |
|
Annotations: C |
|
| 389.2 | 36650.7 |
|
Annotations: ZZ |
|
| 389.9 | 212.3 |
| 407.1 | 16586.3 |
|
Annotations: ZY |
|
| 407.9 | 1693.7 |
| 408.9 | 13414.7 |
| 409.9 | 4494.7 |
| 423.7 | 3183.0 |
|
Annotations: ^{0,4}A_{GalNAc} |
|
| 424.3 | 3142.0 |
|
Annotations: ^{0,4}A_{GalNAc} |
|
| 427.0 | 4065.7 |
|
Annotations: ^{0,2}A_{GlcNAc} |
|
| 437.9 | 1113.0 |
|
Annotations: ^{3,5}A_{GalNAc} |
|
| 442.1 | 5287.0 |
| 443.0 | 2025.7 |
| 467.0 | 2128.7 |
| 467.8 | 2499.7 |
| 479.0 | 579.3 |
| 508.9 | 4211.0 |
| 510.2 | 5701.3 |
|
Annotations: B |
|
| 511.0 | 819.0 |
| 521.0 | 4352.7 |
| 521.6 | 1811.0 |
| 527.0 | 18770.7 |
| 528.1 | 7943.0 |
|
Annotations: C |
|
| 532.4 | 830.3 |
| 540.6 | 1469.3 |
| 545.3 | 2203.0 |
| 550.0 | 876.3 |
| 551.2 | 11565.7 |
|
Annotations: ZZ |
|
| 552.1 | 1570.0 |
| 560.4 | 5014.0 |
| 569.1 | 288524.0 |
|
Annotations: Z |
|
| 570.1 | 28126.7 |
|
Annotations: ^{2,4}A_{GalNAc} |
|
| 574.1 | 1762.7 |
| 587.0 | 32187.0 |
|
Annotations: Y |
|
| 587.7 | 1.3 |
|
Annotations: Y |
|
| 592.1 | 18229.3 |
|
Annotations: ZZ |
|
| 592.9 | 2500.7 |
| 609.9 | 8836.7 |
|
Annotations: ZY |
|
| 625.0 | 9785.3 |
| 645.9 | 1629.7 |
| 652.0 | 655.0 |
| 681.9 | 1356.7 |
| 691.3 | 2243.7 |
| 694.9 | 3458.3 |
| 712.4 | 6792.7 |
| 715.0 | 6613.0 |
|
Annotations: Z |
|
| 715.9 | 7634.7 |
| 724.2 | 1962.3 |
|
Annotations: ^{1,5}A_{GalNAc}Z |
|
| 730.3 | 5932.3 |
| 733.3 | 3896.7 |
|
Annotations: Y |
|
| 753.8 | 366.7 |
|
Annotations: ZZ |
|
| 756.6 | 1087.3 |
| 772.2 | 135497.3 |
|
Annotations: Z |
|
| 773.1 | 28127.0 |
| 790.1 | 1005.0 |
|
Annotations: Y |
|
| 795.6 | 161.7 |
| 834.4 | 4400.3 |
| 837.3 | 6733.7 |
| 841.8 | 4617.0 |
| 857.9 | 1681.7 |
| 858.5 | 850.0 |
| 875.0 | 2384.0 |
| 876.2 | 3311.3 |
| 892.7 | 1060.3 |
| 894.2 | 6842.3 |
| 895.3 | 7636.7 |
| 898.1 | 1189.3 |
| 900.1 | 2860.3 |
| 901.2 | 6806.3 |
| 918.2 | 23376.7 |
|
Annotations: Z |
|
| 919.1 | 4487.3 |
| 930.1 | 2312.7 |
| 933.9 | 1229.3 |
|
Annotations: Z |
|
| 935.0 | 4082.0 |
| 936.3 | 17217.3 |
|
Annotations: Y |
|
| 937.2 | 2214.0 |
| 953.2 | 804.0 |
| 978.4 | 4123.7 |
| 978.9 | 1011.0 |
|
Annotations: ^{2,5}A_{GalNAc} |
|
| 983.6 | 3322.3 |
| 996.4 | 3567.3 |
| 997.2 | 4200.7 |
| 1015.1 | 426.0 |
| 1038.1 | 37442.7 |
| 1039.3 | 15455.3 |
| 1054.6 | 1201.7 |
| 1056.2 | 60818.3 |
| 1057.1 | 6095.3 |
| 1137.2 | 1441.7 |
| 1212.2 | 557.0 |