Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.
GlyToucan Accession Number: G91731DX
| Peak | Intensity |
|---|---|
| 288.8 | 211.9 |
| 298.8 | 1999.3 |
| 306.1 | 2232.8 |
| 306.8 | 4612.9 |
|
Annotations: B |
|
| 307.8 | 1626.1 |
| 324.6 | 25839.8 |
| 328.7 | 381.0 |
| 346.0 | 7146.0 |
|
Annotations: BZ |
|
| 347.0 | 808.8 |
| 353.3 | 87.0 |
| 364.9 | 160.4 |
| 367.1 | 11416.6 |
|
Annotations: ^{2,4}A_{GalNAc} |
|
| 370.1 | 701.8 |
| 370.7 | 2833.4 |
| 388.9 | 77233.1 |
|
Annotations: ZZ |
|
| 390.0 | 4276.1 |
| 392.0 | 594.6 |
| 406.2 | 1511.0 |
|
Annotations: ^{0,4}A_{GalNAc}Z |
|
| 407.1 | 19367.8 |
|
Annotations: YZ |
|
| 408.2 | 11028.8 |
|
Annotations: ^{1,3}A_{GalNAc} |
|
| 408.8 | 64077.6 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 409.4 | 5.1 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 443.4 | 901.8 |
| 450.7 | 446.3 |
| 451.5 | 1428.6 |
| 452.0 | 419.0 |
| 461.0 | 1030.5 |
| 467.4 | 709.1 |
| 479.1 | 1532.8 |
| 486.9 | 905.6 |
| 490.9 | 319.4 |
| 491.9 | 906.1 |
| 503.2 | 125.5 |
| 506.0 | 1408.3 |
| 508.9 | 5093.4 |
| 510.1 | 11365.5 |
|
Annotations: B |
|
| 510.9 | 214.0 |
| 512.1 | 13238.6 |
|
Annotations: Z |
|
| 526.9 | 1275.6 |
| 527.9 | 1611.1 |
|
Annotations: C |
|
| 530.0 | 2058.9 |
|
Annotations: Y |
|
| 550.9 | 41927.8 |
|
Annotations: ZZ |
|
| 552.0 | 8181.4 |
| 552.7 | 299.0 |
| 557.9 | 462.9 |
| 566.1 | 90.3 |
| 568.8 | 14548.9 |
|
Annotations: YZ |
|
| 569.4 | 1083.1 |
|
Annotations: YZ |
|
| 570.1 | 22194.8 |
|
Annotations: ^{0,4}A_{GalNAc} |
|
| 571.1 | 845.5 |
| 584.3 | 1356.4 |
|
Annotations: ^{3,5}A_{GalNAc} |
|
| 588.3 | 877.1 |
| 595.1 | 1907.6 |
| 596.0 | 2031.3 |
|
Annotations: ^{2,5}A_{GalNAc}Z |
|
| 611.9 | 1336.5 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 612.6 | 1470.5 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 614.0 | 2003.4 |
|
Annotations: ^{2,5}A_{GalNAc}Y |
|
| 620.6 | 364.8 |
| 630.4 | 2028.9 |
|
Annotations: ^{0,2}A_{GalNAc}Y |
|
| 630.9 | 168.6 |
| 655.2 | 23400.0 |
| 656.1 | 2396.8 |
| 667.3 | 5400.1 |
|
Annotations: ^{1,5}A_{GalNAc}Z |
|
| 673.1 | 102424.8 |
| 674.3 | 8595.1 |
| 679.2 | 694.4 |
| 690.9 | 3022.8 |
| 691.5 | 4297.4 |
| 696.6 | 181.6 |
| 697.1 | 12638.0 |
| 698.0 | 1137.6 |
| 712.5 | 94.4 |
| 714.4 | 1039.9 |
| 715.1 | 779577.5 |
|
Annotations: Z |
|
| 716.1 | 121531.5 |
| 716.9 | 0.1 |
| 729.1 | 4501.3 |
| 733.1 | 17636.1 |
|
Annotations: Y |
|
| 733.9 | 318.1 |
| 741.5 | 421.8 |
| 749.0 | 825.8 |
|
Annotations: YY |
|
| 751.2 | 70.3 |
| 755.0 | 1971.1 |
| 757.3 | 1637.8 |
| 765.3 | 196.3 |
| 772.1 | 1641.6 |
| 775.1 | 1738.8 |
| 784.2 | 150.3 |
| 793.4 | 288.4 |
| 795.0 | 218.3 |
| 801.4 | 78.5 |
| 803.8 | 180.5 |
| 810.9 | 2350.0 |
| 817.1 | 640.0 |
| 817.7 | 7523.8 |
| 824.2 | 588.9 |
| 827.2 | 303.8 |
| 834.7 | 230.8 |
| 835.5 | 2906.3 |
| 837.4 | 254.1 |
| 853.2 | 8529.5 |
| 861.0 | 323.5 |
| 862.3 | 611.5 |
| 876.1 | 1199.3 |
| 877.3 | 8857.1 |
|
Annotations: Z |
|
| 878.2 | 1412.1 |
| 879.3 | 3141.4 |
| 880.3 | 87.0 |
| 895.0 | 9789.9 |
|
Annotations: Y |
|
| 895.8 | 70.6 |
|
Annotations: Y |
|
| 899.0 | 2868.1 |
| 902.8 | 69.5 |
| 904.3 | 230.0 |
| 905.6 | 3342.4 |
| 910.9 | 753.4 |
| 912.1 | 162.5 |
| 920.4 | 306.5 |
| 921.0 | 2778.9 |
| 927.7 | 103.3 |
| 939.1 | 10755.4 |
| 940.7 | 382.1 |
| 946.8 | 769.1 |
| 962.4 | 162.5 |
| 967.3 | 141.5 |
| 968.3 | 848.9 |
| 980.1 | 2729.5 |
| 981.2 | 58480.8 |
| 981.7 | 0.1 |
| 982.3 | 35180.1 |
| 989.2 | 976.5 |
| 992.3 | 970.4 |
| 997.9 | 84.0 |
| 999.2 | 91237.9 |
| 1000.3 | 20609.4 |
| 1001.2 | 837.3 |
| 1001.8 | 763.8 |
| 1011.3 | 4076.1 |
| 1019.7 | 982.0 |
| 1021.1 | 135.5 |
| 1022.9 | 163.5 |
| 1060.3 | 2074.3 |
| 1082.3 | 58.6 |
| 1089.5 | 242.8 |
| 1112.3 | 146.3 |
| 1176.3 | 702.9 |
| 1177.2 | 271.1 |
| 1184.3 | 978.8 |
| 1193.1 | 825.0 |