Efficient Chemoenzymatic Synthesis of an N-glycan Isomer Library
Peak | Intensity |
---|---|
163.19 | 0.1 |
Annotations: B |
|
168.1 | 2.1 |
173.07 | 0.2 |
174.21 | 0.1 |
181.27 | 0.1 |
Annotations: C |
|
186.12 | 3.9 |
Annotations: BZ |
|
194.94 | 0.1 |
204.09 | 81.1 |
Annotations: Z B Z |
|
205.06 | 2.5 |
Annotations: ^{0,4}A_{Man}Z |
|
221.3 | 0.2 |
Annotations: ^{1,5}A_{Man}Z |
|
222.16 | 3.8 |
Annotations: C Y |
|
223.19 | 0.4 |
Annotations: ^{0,2}A_{Man}Y ^{0,4}A_{Man}Y ^{1,3}A_{Man} ^{2,4}A_{Man} |
|
226.18 | 0.1 |
242.05 | 0.3 |
245.93 | 0.1 |
247.2 | 0.1 |
252.22 | 0.1 |
262.34 | 0.2 |
276.05 | 0.2 |
Annotations: ZZ |
|
285.51 | 0.2 |
Annotations: ZY YZ |
|
289.26 | 0.1 |
291.18 | 0.1 |
292.38 | 0.1 |
293.17 | 0.3 |
300.02 | 0.1 |
300.54 | 0.1 |
301.26 | 0.2 |
306.17 | 0.2 |
307.32 | 0.1 |
Annotations: BZ |
|
309.12 | 0.1 |
310.32 | 0.1 |
314.88 | 0.4 |
318.13 | 0.1 |
321.23 | 0.2 |
323.13 | 0.1 |
325.08 | 0.3 |
Annotations: BY CZ |
|
326.31 | 0.1 |
335.24 | 0.1 |
337.03 | 0.1 |
Annotations: BZ |
|
338.24 | 0.2 |
Annotations: ^{1,5}A_{Man} |
|
340.93 | 0.1 |
342.06 | 0.2 |
342.88 | 0.2 |
Annotations: CY |
|
343.92 | 0.3 |
346.18 | 0.1 |
353.28 | 0.1 |
354.19 | 0.3 |
Annotations: C |
|
355.11 | 0.3 |
Annotations: C |
|
356.75 | 0.2 |
Annotations: BZ ZZ |
|
357.48 | 0.3 |
Annotations: BZ ZZ |
|
361.39 | 0.1 |
364.61 | 1.0 |
366.23 | 23.9 |
Annotations: B Z |
|
367.18 | 1.4 |
367.88 | 0.2 |
374.22 | 0.2 |
377.11 | 0.1 |
378.03 | 0.1 |
384.26 | 0.2 |
Annotations: C |
|
386.53 | 0.1 |
387.12 | 0.1 |
388.27 | 0.2 |
388.86 | 0.1 |
390.27 | 0.2 |
392.1 | 0.2 |
393.11 | 0.2 |
394.53 | 0.5 |
395.42 | 1.2 |
396.2 | 0.3 |
397.92 | 0.1 |
399.24 | 0.2 |
402.17 | 0.2 |
404.05 | 0.1 |
404.67 | 0.4 |
405.99 | 0.5 |
407.27 | 0.5 |
Annotations: Z |
|
408.44 | 0.1 |
408.96 | 0.1 |
413.35 | 0.2 |
417.31 | 0.2 |
419.14 | 0.1 |
420.27 | 0.3 |
421.28 | 0.2 |
422.97 | 0.5 |
425.17 | 2.5 |
Annotations: Y |
|
426.17 | 0.3 |
Annotations: ^{0,4}A_{Man} |
|
426.88 | 0.1 |
Annotations: ^{0,2}A_{Man}Z |
|
427.97 | 0.1 |
429.09 | 0.2 |
Annotations: ^{2,5}A_{Man}Y |
|
430.61 | 0.4 |
432.25 | 0.1 |
436.12 | 0.2 |
437.09 | 0.4 |
438.27 | 0.8 |
440.02 | 0.1 |
Annotations: ^{3,5}A_{Man} |
|
441.94 | 0.1 |
442.63 | 0.1 |
445.11 | 0.6 |
Annotations: ^{0,2}A_{Man}Y |
|
446.46 | 1.1 |
447.31 | 1.8 |
Annotations: B Z |
|
448.12 | 0.1 |
450.95 | 0.1 |
451.52 | 0.1 |
454.2 | 0.3 |
455.32 | 0.8 |
455.93 | 0.1 |
Annotations: C Y |
|
456.63 | 0.1 |
Annotations: C Y |
|
457.54 | 0.1 |
458.17 | 0.4 |
459.04 | 0.5 |
Annotations: ^{1,5}A_{Man}Y |
|
459.93 | 0.2 |
460.95 | 0.4 |
462.14 | 0.3 |
463.27 | 0.2 |
464.14 | 0.2 |
465.11 | 0.6 |
466.08 | 0.8 |
466.83 | 0.5 |
467.84 | 14.8 |
Annotations: Z |
|
468.41 | 0.6 |
469.02 | 0.2 |
Annotations: BZ |
|
469.55 | 0.1 |
Annotations: BZ |
|
471.86 | 0.1 |
473.44 | 0.1 |
474.06 | 0.1 |
475.6 | 2.8 |
476.8 | 29.3 |
Annotations: Y |
|
477.42 | 1.0 |
478.02 | 2.9 |
479.06 | 0.4 |
480.1 | 0.1 |
480.91 | 0.4 |
482.24 | 0.1 |
483.26 | 0.3 |
484.12 | 0.1 |
485.32 | 0.2 |
486.03 | 0.4 |
486.87 | 0.2 |
Annotations: BY CZ |
|
487.64 | 0.1 |
Annotations: BY CZ |
|
489.2 | 0.1 |
491.17 | 0.2 |
491.9 | 0.1 |
493.23 | 0.7 |
494.69 | 1.0 |
496.21 | 0.5 |
497.12 | 1.4 |
498.2 | 0.3 |
499.0 | 0.8 |
500.23 | 0.1 |
501.14 | 0.4 |
503.54 | 0.3 |
506.3 | 0.1 |
507.21 | 0.2 |
508.08 | 0.2 |
509.11 | 0.3 |
510.1 | 0.2 |
Annotations: BZ BZ |
|
510.96 | 0.4 |
512.06 | 0.5 |
513.18 | 0.6 |
513.88 | 0.1 |
515.09 | 0.1 |
517.14 | 0.2 |
519.12 | 0.5 |
520.01 | 0.6 |
521.18 | 2.1 |
522.0 | 4.1 |
522.96 | 0.6 |
524.18 | 0.1 |
525.61 | 0.3 |
526.91 | 1.5 |
528.3 | 29.4 |
Annotations: BY CZ BY CZ |
|
529.3 | 3.1 |
530.33 | 0.2 |
530.9 | 0.1 |
534.93 | 0.2 |
537.09 | 0.3 |
537.6 | 0.4 |
538.29 | 0.1 |
539.15 | 2.9 |
539.96 | 0.7 |
540.61 | 1.6 |
541.25 | 0.5 |
542.48 | 0.4 |
546.39 | 0.3 |
Annotations: CY CY |
|
547.52 | 0.7 |
548.75 | 2.9 |
549.35 | 0.9 |
551.63 | 0.1 |
Annotations: ZZ |
|
553.63 | 0.1 |
556.88 | 0.5 |
557.89 | 0.1 |
558.77 | 0.7 |
559.52 | 0.2 |
569.36 | 3.3 |
Annotations: ZY YZ |
|
570.35 | 0.6 |
573.71 | 0.3 |
575.97 | 0.2 |
577.93 | 0.1 |
581.71 | 0.1 |
584.66 | 0.1 |
585.24 | 0.1 |
586.37 | 0.7 |
587.37 | 14.4 |
Annotations: YY |
|
588.32 | 1.2 |
589.44 | 0.5 |
590.82 | 0.1 |
594.43 | 0.2 |
601.72 | 0.2 |
602.27 | 0.3 |
628.15 | 0.2 |
648.9 | 0.2 |
654.27 | 0.1 |
655.88 | 0.1 |
672.17 | 0.1 |
Annotations: BZ |
|
682.87 | 0.1 |
683.66 | 0.2 |
684.24 | 0.1 |
688.42 | 0.5 |
689.51 | 1.3 |
690.39 | 31.7 |
Annotations: B |
|
691.36 | 4.6 |
692.58 | 0.1 |
708.36 | 0.1 |
Annotations: C |
|
713.48 | 0.2 |
Annotations: BZ ZZ |
|
714.57 | 0.1 |
716.18 | 0.2 |
727.27 | 0.3 |
728.35 | 0.1 |
729.45 | 0.7 |
730.45 | 0.8 |
731.41 | 33.4 |
Annotations: Z |
|
732.42 | 4.3 |
734.31 | 0.2 |
736.18 | 0.4 |
744.27 | 0.3 |
747.1 | 0.1 |
747.72 | 1.6 |
748.56 | 0.9 |
749.4 | 90.2 |
Annotations: Y |
|
750.38 | 9.0 |
751.51 | 0.2 |
754.43 | 0.3 |
755.38 | 0.1 |
756.53 | 0.5 |
760.82 | 0.1 |
764.69 | 0.3 |
770.1 | 0.1 |
788.36 | 0.1 |
851.57 | 0.2 |
858.18 | 0.1 |
876.39 | 0.2 |
883.34 | 0.1 |
891.57 | 0.5 |
892.58 | 0.9 |
893.47 | 35.6 |
Annotations: B Z |
|
894.46 | 5.7 |
897.31 | 0.1 |
908.44 | 0.1 |
909.26 | 0.9 |
910.32 | 2.2 |
910.88 | 0.4 |
Annotations: C Y |
|
911.45 | 163.2 |
Annotations: C Y |
|
912.46 | 28.3 |
913.23 | 0.9 |
913.93 | 0.4 |
918.38 | 0.1 |
931.53 | 0.2 |
932.43 | 0.1 |
934.15 | 0.2 |
Annotations: Z |
|
934.8 | 0.1 |
Annotations: Z |
|
947.43 | 0.1 |
951.67 | 0.2 |
952.46 | 0.9 |
Annotations: Y |
|
953.22 | 0.2 |
955.49 | 0.3 |
974.5 | 0.4 |
1034.7 | 0.2 |
1035.24 | 0.1 |
1058.58 | 0.1 |
1075.67 | 0.1 |
1092.44 | 0.2 |
1094.58 | 1.2 |
1095.33 | 0.3 |
1105.47 | 0.1 |