Efficient Chemoenzymatic Synthesis of an N-glycan Isomer Library
Peak | Intensity |
---|---|
167.34 | 0.1 |
168.05 | 5.2 |
174.11 | 0.1 |
181.99 | 0.2 |
186.1 | 5.4 |
Annotations: BZ |
|
189.32 | 0.1 |
199.25 | 0.1 |
200.84 | 0.1 |
203.14 | 0.4 |
204.09 | 95.5 |
Annotations: Z B Z |
|
205.07 | 4.2 |
Annotations: ^{1,3}A_{Man}Z ^{2,4}A_{Man}Z |
|
206.13 | 0.1 |
Annotations: ^{2,5}A_{Man}Z |
|
216.45 | 0.2 |
217.01 | 0.3 |
221.24 | 0.2 |
Annotations: ^{1,5}A_{Man}Z |
|
222.13 | 4.3 |
Annotations: C Y |
|
222.87 | 0.2 |
Annotations: ^{1,3}A_{Man}Y ^{2,4}A_{Man}Y ^{0,2}A_{Man}Y ^{0,4}A_{Man} |
|
225.24 | 0.1 |
236.12 | 0.1 |
244.99 | 0.1 |
246.17 | 0.1 |
247.27 | 0.2 |
254.01 | 0.1 |
256.79 | 0.2 |
263.02 | 0.1 |
263.97 | 0.2 |
Annotations: ^{1,3}A_{Man} |
|
269.15 | 0.1 |
273.3 | 0.2 |
Annotations: CY CY |
|
276.97 | 0.1 |
283.38 | 0.6 |
292.07 | 0.1 |
295.03 | 0.1 |
301.03 | 0.1 |
305.55 | 0.2 |
312.12 | 0.1 |
314.82 | 0.4 |
315.99 | 0.1 |
317.02 | 0.2 |
Annotations: ^{2,5}A_{Man} |
|
318.15 | 0.1 |
325.21 | 0.1 |
Annotations: BY CZ |
|
327.39 | 0.2 |
333.46 | 0.2 |
336.12 | 0.1 |
342.98 | 0.2 |
Annotations: CY |
|
344.07 | 0.1 |
344.98 | 0.2 |
348.13 | 0.4 |
355.03 | 0.2 |
Annotations: C |
|
356.02 | 0.4 |
356.83 | 0.2 |
Annotations: BZ ZZ |
|
362.98 | 0.2 |
365.01 | 0.7 |
365.53 | 0.1 |
366.23 | 31.2 |
Annotations: B Z |
|
367.17 | 1.2 |
367.91 | 0.1 |
370.29 | 0.2 |
374.37 | 0.2 |
375.18 | 0.3 |
Annotations: Y |
|
377.07 | 0.1 |
378.15 | 0.3 |
379.89 | 0.1 |
382.16 | 0.1 |
383.11 | 0.2 |
384.09 | 0.2 |
Annotations: C |
|
385.31 | 0.1 |
388.03 | 0.3 |
394.17 | 0.2 |
396.0 | 1.2 |
398.38 | 0.3 |
400.39 | 0.1 |
401.14 | 0.2 |
402.39 | 0.1 |
402.99 | 0.1 |
403.98 | 0.1 |
404.99 | 0.4 |
407.17 | 0.5 |
Annotations: Z |
|
407.79 | 0.1 |
409.24 | 0.1 |
413.03 | 0.1 |
414.31 | 0.3 |
419.11 | 0.3 |
420.18 | 0.1 |
423.06 | 0.7 |
425.29 | 2.8 |
Annotations: Y |
|
426.14 | 0.2 |
Annotations: ^{1,3}A_{Man} ^{2,4}A_{Man} |
|
427.36 | 0.1 |
Annotations: ^{0,2}A_{Man}Z |
|
428.3 | 1.2 |
429.14 | 0.3 |
Annotations: ^{2,5}A_{Man}Y |
|
430.07 | 0.2 |
431.17 | 0.4 |
431.99 | 1.1 |
433.07 | 0.1 |
436.27 | 0.3 |
441.85 | 0.1 |
444.08 | 0.2 |
447.3 | 10.1 |
Annotations: B Z |
|
448.11 | 0.4 |
448.7 | 0.1 |
451.16 | 0.1 |
455.39 | 0.3 |
456.28 | 0.5 |
Annotations: C Y |
|
458.09 | 0.3 |
459.06 | 0.2 |
Annotations: ^{1,5}A_{Man}Y |
|
463.12 | 0.1 |
463.74 | 0.1 |
465.12 | 0.6 |
466.22 | 0.4 |
467.04 | 0.3 |
467.81 | 8.2 |
Annotations: Z |
|
468.53 | 0.6 |
469.09 | 0.3 |
Annotations: BZ |
|
470.14 | 0.2 |
473.0 | 0.4 |
473.95 | 0.1 |
475.79 | 1.0 |
476.81 | 15.4 |
Annotations: Y |
|
477.34 | 0.2 |
477.92 | 3.5 |
478.87 | 0.6 |
480.05 | 0.4 |
481.09 | 0.4 |
482.03 | 0.7 |
483.07 | 0.9 |
483.97 | 0.2 |
485.05 | 0.3 |
485.98 | 0.3 |
487.27 | 0.1 |
Annotations: BY CZ |
|
488.14 | 0.2 |
489.09 | 0.3 |
491.02 | 0.3 |
491.79 | 0.1 |
492.31 | 0.1 |
492.99 | 0.2 |
495.05 | 0.3 |
497.19 | 0.6 |
498.03 | 0.5 |
499.07 | 0.1 |
499.9 | 1.3 |
501.6 | 0.2 |
503.31 | 0.6 |
503.93 | 0.1 |
504.69 | 0.7 |
Annotations: CY |
|
505.48 | 0.1 |
Annotations: CY |
|
507.05 | 0.2 |
508.66 | 0.2 |
509.18 | 0.3 |
510.04 | 0.9 |
Annotations: BZ BZ |
|
511.14 | 0.6 |
511.95 | 0.2 |
512.9 | 0.6 |
513.93 | 0.2 |
515.98 | 0.1 |
516.69 | 0.4 |
517.82 | 0.5 |
518.96 | 0.3 |
520.01 | 0.4 |
521.16 | 2.2 |
522.01 | 3.1 |
522.74 | 0.2 |
524.86 | 0.3 |
525.58 | 0.1 |
526.66 | 0.4 |
527.27 | 0.3 |
528.29 | 34.0 |
Annotations: BY CZ BY CZ |
|
529.34 | 3.2 |
530.46 | 0.7 |
535.44 | 0.1 |
536.82 | 0.2 |
538.17 | 0.3 |
538.99 | 2.3 |
540.06 | 1.7 |
541.12 | 0.8 |
541.95 | 0.6 |
542.77 | 0.2 |
544.17 | 0.1 |
544.68 | 0.2 |
545.62 | 0.3 |
546.34 | 0.3 |
Annotations: CY CY |
|
547.48 | 0.4 |
548.03 | 0.4 |
548.9 | 6.4 |
549.57 | 0.5 |
556.79 | 0.2 |
557.69 | 0.1 |
558.91 | 0.5 |
564.55 | 0.3 |
567.69 | 0.1 |
569.28 | 2.1 |
Annotations: YZ ZY |
|
570.21 | 0.7 |
571.39 | 0.1 |
574.3 | 0.2 |
586.4 | 0.1 |
587.37 | 13.7 |
Annotations: YY |
|
588.26 | 1.4 |
591.17 | 0.1 |
610.25 | 0.2 |
610.92 | 0.4 |
634.5 | 0.1 |
641.29 | 0.2 |
644.24 | 0.3 |
657.43 | 0.1 |
672.12 | 0.1 |
Annotations: BZ |
|
673.38 | 0.1 |
675.37 | 0.2 |
681.68 | 0.1 |
682.9 | 0.4 |
688.61 | 0.3 |
689.53 | 0.8 |
690.38 | 50.9 |
Annotations: B |
|
691.39 | 7.1 |
694.38 | 0.1 |
696.27 | 0.2 |
697.9 | 0.1 |
703.52 | 0.3 |
705.37 | 0.1 |
707.73 | 0.1 |
708.33 | 0.7 |
Annotations: C |
|
709.38 | 0.1 |
710.09 | 0.1 |
714.99 | 0.2 |
726.26 | 0.2 |
729.66 | 0.2 |
730.55 | 0.7 |
731.44 | 26.4 |
Annotations: Z |
|
732.5 | 4.1 |
733.11 | 0.2 |
735.67 | 0.3 |
747.61 | 0.7 |
748.5 | 1.3 |
749.41 | 78.3 |
Annotations: Y |
|
750.42 | 14.3 |
750.93 | 0.1 |
788.46 | 0.1 |
802.29 | 0.2 |
852.87 | 0.1 |
861.5 | 0.1 |
876.19 | 0.2 |
891.25 | 0.3 |
892.0 | 0.5 |
892.67 | 0.6 |
893.47 | 47.4 |
Annotations: B Z |
|
894.45 | 8.5 |
895.36 | 0.7 |
907.58 | 0.1 |
908.45 | 0.1 |
909.04 | 0.3 |
910.0 | 3.4 |
910.72 | 3.8 |
911.45 | 180.5 |
Annotations: C Y |
|
912.46 | 37.5 |
913.18 | 0.5 |
914.66 | 0.2 |
934.41 | 0.1 |
Annotations: Z |
|
952.73 | 0.3 |
Annotations: Y |
|
963.59 | 0.2 |
964.39 | 0.1 |