Efficient Chemoenzymatic Synthesis of an N-glycan Isomer Library
Peak | Intensity |
---|---|
185.2 | 0.6 |
186.1 | 134.7 |
Annotations: BZ BZ |
|
187.11 | 1.4 |
204.06 | 1439.4 |
Annotations: Z Z |
|
205.15 | 55.7 |
Annotations: ^{0,4}A_{Man}Z |
|
222.13 | 249.3 |
Annotations: Y |
|
223.15 | 13.3 |
Annotations: ^{2,4}A_{GlcNAc} ^{0,2}A_{Man}Y ^{0,4}A_{Man}Y ^{1,3}A_{Man} ^{2,4}A_{Man} |
|
228.14 | 1.9 |
Annotations: ^{1,4}A_{Man} ^{0,3}A_{Man}Y |
|
241.21 | 1.2 |
247.23 | 0.3 |
269.2 | 1.2 |
289.12 | 0.9 |
300.19 | 1.9 |
305.9 | 4.0 |
312.08 | 0.7 |
314.75 | 0.7 |
324.41 | 0.5 |
Annotations: ^{0,2}A_{Man}Y |
|
325.22 | 8.9 |
Annotations: BY CZ |
|
326.37 | 1.6 |
330.12 | 11.0 |
331.08 | 0.4 |
343.15 | 1.2 |
Annotations: CY |
|
348.18 | 19.3 |
Annotations: BZ |
|
354.17 | 1.7 |
Annotations: CY CY CY |
|
362.09 | 1.2 |
364.63 | 4.7 |
365.35 | 28.3 |
366.15 | 7851.0 |
Annotations: B Z |
|
367.17 | 643.4 |
367.87 | 8.6 |
371.96 | 2.5 |
384.15 | 8.2 |
Annotations: C |
|
385.4 | 4.2 |
386.68 | 0.6 |
389.24 | 1.6 |
393.78 | 1.8 |
395.94 | 9.5 |
404.84 | 1.6 |
406.41 | 3.3 |
407.33 | 45.7 |
Annotations: Z |
|
408.13 | 2.5 |
Annotations: ^{0,4}A_{Man}Z |
|
409.28 | 0.8 |
410.79 | 1.8 |
Annotations: ^{2,5}A_{Man}Z |
|
416.0 | 1.5 |
418.17 | 1.3 |
423.82 | 1.6 |
424.38 | 1.2 |
425.25 | 207.0 |
Annotations: Y |
|
426.3 | 17.5 |
Annotations: B |
|
427.3 | 0.6 |
Annotations: ^{0,2}A_{Man}Z |
|
429.22 | 3.5 |
Annotations: ^{2,5}A_{Man}Y |
|
438.22 | 5.3 |
Annotations: BZ BZ |
|
446.58 | 4.2 |
447.29 | 909.2 |
Annotations: Z |
|
447.95 | 22.0 |
449.2 | 1.2 |
451.28 | 1.4 |
456.27 | 4.2 |
Annotations: Y |
|
457.88 | 1.3 |
459.03 | 2.5 |
Annotations: ZZ |
|
466.36 | 1.2 |
467.83 | 238.9 |
Annotations: ZY YZ |
|
468.7 | 5.0 |
Annotations: BZ |
|
473.38 | 4.3 |
475.49 | 9.5 |
476.84 | 266.9 |
Annotations: YY |
|
477.66 | 19.0 |
478.54 | 2.4 |
479.47 | 2.5 |
481.93 | 0.3 |
486.24 | 0.7 |
487.17 | 3.2 |
Annotations: BY CZ |
|
488.3 | 0.4 |
492.18 | 2.2 |
503.5 | 1.0 |
505.23 | 1.0 |
Annotations: CY |
|
510.18 | 0.4 |
Annotations: BZ |
|
519.8 | 1.9 |
526.07 | 12.2 |
527.25 | 38.4 |
528.22 | 4566.2 |
Annotations: B B |
|
529.22 | 488.5 |
529.79 | 3.6 |
530.72 | 5.0 |
531.38 | 1.8 |
533.21 | 0.9 |
534.97 | 0.7 |
537.22 | 6.7 |
Annotations: C |
|
539.67 | 13.5 |
540.36 | 1.1 |
541.22 | 1.2 |
546.28 | 25.7 |
Annotations: C |
|
547.94 | 17.7 |
548.86 | 590.4 |
Annotations: Z Z |
|
549.37 | 27.4 |
549.89 | 6.4 |
551.23 | 5.5 |
Annotations: ZZ |
|
555.11 | 0.7 |
555.64 | 3.1 |
556.85 | 39.4 |
557.82 | 1863.8 |
Annotations: Y Y |
|
558.43 | 94.6 |
559.01 | 18.6 |
560.86 | 4.0 |
561.93 | 1.5 |
563.88 | 2.5 |
565.18 | 2.7 |
566.11 | 2.4 |
567.22 | 3.3 |
568.44 | 2.0 |
569.29 | 302.3 |
Annotations: ZY YZ |
|
570.3 | 18.4 |
571.93 | 1.7 |
574.89 | 2.7 |
576.26 | 0.9 |
585.44 | 7.1 |
586.59 | 2.6 |
587.29 | 747.3 |
Annotations: YY |
|
588.29 | 102.2 |
Annotations: ^{0,4}A_{Man} |
|
594.47 | 0.3 |
611.8 | 3.8 |
613.28 | 2.1 |
621.05 | 15.2 |
623.17 | 2.6 |
628.22 | 2.0 |
628.8 | 3.9 |
629.79 | 53.0 |
Annotations: ^{0,2}A_{Man}Z |
|
630.45 | 1.9 |
Annotations: ^{0,2}A_{Man}Z |
|
638.76 | 4.6 |
654.33 | 7.0 |
672.34 | 8.5 |
Annotations: BZ BZ BZ |
|
673.33 | 1.4 |
677.37 | 3.0 |
688.51 | 8.2 |
689.55 | 30.1 |
690.29 | 2366.5 |
Annotations: BY CZ CZ BY CZ BY |
|
691.31 | 371.4 |
692.03 | 4.3 |
693.01 | 1.4 |
696.21 | 2.6 |
707.74 | 0.6 |
708.4 | 28.8 |
Annotations: CY CY CY |
|
709.27 | 1.4 |
713.28 | 16.7 |
Annotations: ZZ |
|
714.08 | 0.6 |
729.21 | 3.8 |
729.98 | 5.7 |
730.65 | 6.1 |
731.32 | 1506.9 |
Annotations: Z |
|
732.32 | 267.8 |
733.28 | 5.5 |
746.54 | 2.7 |
747.35 | 20.6 |
748.34 | 85.6 |
749.3 | 3715.9 |
Annotations: Y |
|
750.34 | 632.0 |
751.06 | 10.9 |
752.28 | 1.6 |
773.22 | 3.0 |
780.13 | 1.1 |
790.37 | 4.8 |
798.31 | 5.2 |
810.62 | 1.0 |
Annotations: ^{0,2}A_{Man} |
|
816.35 | 1.2 |
850.51 | 0.7 |
852.36 | 54.7 |
Annotations: B |
|
853.37 | 8.3 |
857.33 | 1.2 |
858.05 | 5.9 |
869.49 | 2.0 |
870.44 | 5.6 |
Annotations: C |
|
871.28 | 2.2 |
873.78 | 1.0 |
875.42 | 6.8 |
Annotations: BZ BZ |
|
875.95 | 2.1 |
877.43 | 1.8 |
890.72 | 2.8 |
891.98 | 10.8 |
892.68 | 3.6 |
893.36 | 1265.7 |
Annotations: Z |
|
894.36 | 288.8 |
909.67 | 30.6 |
910.58 | 137.3 |
911.34 | 4662.5 |
Annotations: Y |
|
912.38 | 1039.3 |
913.28 | 19.9 |
916.27 | 0.9 |
Annotations: ZZ |
|
933.67 | 0.6 |
934.49 | 25.2 |
Annotations: ZY YZ |
|
935.41 | 6.2 |
952.45 | 23.7 |
Annotations: YY |
|
953.41 | 5.7 |
954.0 | 2.7 |
994.26 | 1.1 |
1002.45 | 0.9 |
1035.53 | 2.5 |
1036.08 | 1.4 |
1037.53 | 3.4 |
1052.56 | 1.7 |
1053.45 | 5.7 |
1054.0 | 0.9 |
1054.58 | 25.4 |
1055.45 | 550.0 |
Annotations: B |
|
1056.43 | 194.8 |
1057.33 | 3.1 |
1072.53 | 3.8 |
1073.49 | 76.7 |
Annotations: C |
|
1074.53 | 21.2 |
1075.67 | 1.5 |
1095.19 | 0.6 |
1096.59 | 12.0 |
Annotations: Z Z |
|
1097.44 | 5.2 |
1114.56 | 17.4 |
Annotations: Y Y |
|
1115.5 | 10.3 |