Efficient Chemoenzymatic Synthesis of an N-glycan Isomer Library

PubMed Entry

Peak Intensity
163.0 2.3

Annotations:

B
167.2 1.2
168.05 752.9
169.09 38.3

Annotations:

^{1,5}A_{Man}Y ^{1,5}A_{GlcNAc}
169.97 2.9

Annotations:

^{1,5}A_{GlcNAc} ^{1,5}A_{Man}Y
172.37 0.2

Annotations:

CY
173.19 0.3
181.6 1.4
184.11 2.4
186.09 352.3

Annotations:

BZ BZ
187.08 22.2
188.03 0.5
195.16 0.9
201.19 1.3
201.99 4.3
202.87 3.6
204.06 2699.7

Annotations:

Z Z
205.11 135.5

Annotations:

^{1,3}A_{Man}Z ^{2,4}A_{Man}Z
205.91 3.3
207.13 0.7
213.07 1.2

Annotations:

Y
220.11 1.3
221.15 1.8
222.11 253.9

Annotations:

Y
222.99 10.0

Annotations:

^{2,4}A_{GlcNAc} ^{1,3}A_{Man}Y ^{2,4}A_{Man}Y
224.4 2.4
225.73 1.3
227.28 0.9
239.28 1.4
241.16 2.6

Annotations:

^{1,5}A_{Man}Z
246.1 1.3

Annotations:

^{1,3}A_{Man}Z
259.11 0.9
264.17 1.0

Annotations:

B
265.26 1.1

Annotations:

^{0,2}A_{Man}Z
269.23 1.2
272.03 0.9
276.25 1.0

Annotations:

^{1,4}A_{Man}Z
280.18 1.7
282.32 1.2
284.56 0.7
285.47 1.9

Annotations:

Z
287.15 2.8
305.11 2.8
306.05 1.8
310.17 0.9
311.18 0.8
313.87 0.8
315.16 0.8
317.11 1.0

Annotations:

^{2,5}A_{Man}
319.1 0.7
322.53 1.3
324.27 1.3

Annotations:

^{0,2}A_{Man}
325.97 1.0
327.9 1.2
329.41 1.1
330.17 15.4
336.16 2.9
340.11 1.3
341.98 1.0
343.94 2.8
345.54 0.9

Annotations:

B
346.17 3.2
348.16 32.3

Annotations:

BZ BZ
349.15 0.8
350.21 4.0
352.1 0.4
357.15 3.9

Annotations:

BZ
357.79 1.1
359.12 0.3
362.56 2.5
363.34 0.7
364.25 57.8
365.21 46.4
366.16 12911.8

Annotations:

B Z
367.18 1142.4
367.91 16.1
369.39 3.5
370.11 1.2
371.08 3.6
372.21 2.2
374.04 0.8
375.34 9.7

Annotations:

Y
381.32 1.5
383.62 0.1
384.22 21.0

Annotations:

C
385.18 6.6
386.74 9.2
389.38 4.6
390.11 1.9
390.9 1.0
394.89 3.1
395.96 8.7
397.24 0.8
398.2 2.4
399.44 1.4
400.28 1.0
401.02 2.0
402.18 0.9
403.72 0.9
405.32 10.1
406.36 0.8
407.27 157.3

Annotations:

Z
408.24 19.3

Annotations:

^{1,3}A_{Man}Z ^{2,4}A_{Man}Z
409.18 0.9
410.36 0.8
411.29 0.8
411.84 2.2
413.29 0.4
414.35 5.7
415.29 0.8
420.3 0.8
421.93 0.8
423.29 6.3
424.29 4.8
425.25 483.5

Annotations:

Y
426.25 57.9

Annotations:

^{1,3}A_{Man}Y ^{1,3}A_{Man} ^{2,4}A_{Man}Y
427.28 3.7
427.95 1.1
428.72 0.6
429.69 3.8
431.28 0.4
432.19 0.8
433.69 1.0
434.26 1.0
435.46 0.7
436.08 1.7
436.99 2.2
438.17 6.7

Annotations:

^{1,4}A_{Man}Z
440.21 0.9
441.93 1.1
444.16 3.1
446.35 68.7
447.26 3142.2

Annotations:

B
447.87 305.3
448.76 12.9
449.89 41.1
452.15 2.0

Annotations:

^{2,5}A_{Man}Z
456.35 152.5

Annotations:

C
456.97 13.5
458.13 13.3
458.68 1.2
459.25 13.0
460.03 2.1
461.19 1.9
462.52 0.2
464.49 1.2
466.11 2.3
466.79 16.1
467.81 659.4

Annotations:

Z
468.36 57.0

Annotations:

^{0,2}A_{Man}Z
468.92 6.4
470.33 2.3

Annotations:

^{2,5}A_{Man}Y
471.33 2.1
472.28 1.1
473.0 1.2
475.12 1.2
475.75 16.2
476.82 144.5

Annotations:

Y
477.93 43.9
479.17 5.1
480.1 3.8
482.21 4.0

Annotations:

^{1,5}A_{Man}Z
484.91 0.8
485.77 1.1

Annotations:

^{0,2}A_{Man}Y
486.5 0.5

Annotations:

^{0,2}A_{Man}Y
487.69 0.9
489.29 4.1
491.04 3.9
492.3 5.4
494.06 0.7
496.18 2.3
497.07 8.1
497.99 2.7
499.07 0.7
504.76 1.7
507.81 0.7
508.98 2.8
510.27 10.9

Annotations:

BZ BZ
511.12 8.3
512.14 2.0
513.19 4.7
514.18 2.8
518.01 0.2
518.96 1.1
521.66 4.2
522.42 1.0
523.96 1.3
525.69 2.3
526.45 19.6
527.15 28.1
528.23 6333.0

Annotations:

B
529.25 1006.8
529.99 9.7
530.57 16.7
533.43 0.7
537.31 0.9
538.26 0.8
539.27 40.7
540.15 22.2
541.28 4.2
542.43 4.6
544.3 2.5
546.3 52.5

Annotations:

C
546.93 2.3
547.8 75.2
548.79 2068.5
549.34 94.6
550.1 9.6
551.09 2.3
553.11 4.0
558.95 1.6
564.27 0.9
567.45 11.6
568.29 12.6
569.3 892.2

Annotations:

Z
570.3 131.5
571.43 3.2
577.11 0.7
584.77 1.2
585.6 15.1
586.41 24.6
587.29 1393.1

Annotations:

Y
588.33 231.1

Annotations:

^{1,3}A_{Man} ^{2,4}A_{Man}
589.18 5.9
590.26 1.8
605.59 1.0
606.21 1.1
608.35 1.6
611.38 0.7
626.38 1.5
627.56 0.2
668.25 0.3
677.31 1.2
681.64 3.2
683.98 0.7
688.95 4.1
690.35 135.5

Annotations:

B
691.33 18.8
692.06 1.0
693.45 0.9
695.22 0.9
695.79 3.0
696.42 3.8
702.43 0.9
706.31 4.4
707.64 4.9
708.34 63.4

Annotations:

C
709.34 15.8
712.61 1.7
713.34 16.5

Annotations:

BZ
714.35 6.2
727.98 2.0
729.51 27.7
730.45 56.7
731.31 5881.3

Annotations:

Z
732.35 1338.0
733.2 30.6
733.75 5.2
741.43 1.2
746.4 7.8
747.63 135.2
748.48 99.8
749.31 7742.1

Annotations:

Y
750.36 1388.6
751.33 43.3
752.13 5.7
753.7 1.6
764.88 1.5
772.57 0.8
774.36 0.6
811.58 1.4
857.47 1.3
858.46 0.9
874.52 1.1
875.37 6.8
876.3 3.3
890.79 2.2
891.58 9.6
892.57 4.4
893.42 438.3

Annotations:

B
894.4 107.3
895.47 6.4
909.32 0.7
910.01 1.4
910.58 4.8
911.44 99.8

Annotations:

C
912.44 19.0
934.43 10.7

Annotations:

Z
935.6 0.9
950.56 0.6
952.48 10.8

Annotations:

Y
953.45 2.6
1076.43 2.0

There are 1 similar spectra:

Id Structure Score

2701

0.99
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