UniCarb-DB

Karlsson NG, Thomsson KA, Glycobiology, 2009, (19): 288 - 300

Retention Time	Recorded Precursor Mass	Structure
29.23	675.0 [M -1H]^1-
44.4	895.3 [M -1H]^1-
44.82	966.0 [M -1H]^1-
47.4	874.0 [M -1H]^1-
47.5	975.5 [M -1H]^1-
48.44	829.4 [M -1H]^1-
48.63	895.3 [M -1H]^1-
50.93	749.3 [M -1H]^1-
51.63	1203.3 [M -1H]^1-
51.8	1186.5 [M -1H]^1-
51.98	1016.5 [M -1H]^1-
53.28	1266.3 [M -1H]^1-
53.49	1041.4 [M -1H]^1-
55.28	1406.6 [M -1H]^1-
55.87	895.3 [M -1H]^1-
56.07	1266.3 [M -1H]^1-
56.16	1040.0 [M -1H]^1-
56.57	1120.0 [M -1H]^1-
56.7	749.3 [M -1H]^1-
57.14	1477.5 [M -1H]^1-
57.5	1186.5 [M -1H]^1-
58.41	1406.6 [M -1H]^1-
61.3	0.0 [M -1H]^1-
61.48	1332.2 [M -1H]^1-
61.78	1041.4 [M -1H]^1-
62.25	1178.5 [M -1H]^1-
63.05	821.26 [M -1H]^1-
63.75	705.4 [M -2H]^2-
63.94	958.6 [M -2H]^2-
64.2	1120.0 [M -1H]^1-
64.39	1260.4 [M -1H]^1-
65.0	1331.0 [M -1H]^1-
65.0	1331.4 [M -1H]^1-
65.95	895.3 [M -1H]^1-
66.24	1186.5 [M -1H]^1-
67.02	1178.5 [M -1H]^1-
67.47	1260.4 [M -1H]^1-
67.79	1771.5 [M -1H]^1-
67.79	885.6 [M -1H]^1-
68.37	1332.2 [M -1H]^1-
69.8	1260.4 [M -1H]^1-
70.05	1121.5 [M -1H]^1-
71.13	1551.5 [M -1H]^1-
71.86	1186.5 [M -1H]^1-
72.19	885.6 [M -1H]^1-
72.19	1771.5 [M -1H]^1-
72.95	1559.57 [M -1H]^1-
73.03	1249.2 [M -2H]^2-
73.33	1625.5 [M -1H]^1-
74.71	812.6 [M -1H]^1-
75.11	1114.4 [M -1H]^1-
75.4	1405.5 [M -1H]^1-
76.52	812.5 [M -2H]^2-
76.52	1625.5 [M -2H]^2-
77.04	1041.4 [M -1H]^1-
77.61	1479.5 [M -1H]^1-
77.61	739.5 [M -2H]^2-
77.92	895.3 [M -1H]^1-
80.42	1479.5 [M -1H]^1-
812.6	812.6 [M -1H]^1-
5267.0	829.0 [M -1H]^1-

Structure Format

SNFG Oxford Text

Biological Context

Taxonomy - Homo Sapiens

Tissue - Saliva

Glycoprotein - Mucin-7

HPLC

Column Custom made Hypercarb Carbon Clad Zirkonium

Method

60 gradient with 10 run rate
10mM Ammonium Bicarbonate
80% Acetonitrile in 10mM Ammonium Bicarbonate

Mass Spec

Thermo Fisher XP ESI