Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.

PubMed Entry

GlyToucan Accession Number: G54043EU

Peak Intensity
407.0 5368.3

Annotations:

ZY YZ
424.9 3507.0

Annotations:

YY
474.1 4072.3
484.0 2212.7
486.0 2651.3
501.8 1678.7
508.9 7293.7
509.8 7798.0

Annotations:

B
525.7 2546.7
551.9 3318.3

Annotations:

^{0,4}A_{GalNAc}Z ^{0,4}A_{GalNAc}Z
574.1 2307.0
587.2 1515.7

Annotations:

YY
591.9 5476.7
595.1 1786.0
625.2 1998.3
656.1 15370.0

Annotations:

B
673.0 18397.7
673.6 0.3
676.3 1327.3
690.2 727.0
690.8 2352.3
697.1 6231.0

Annotations:

ZZ ZZ
715.0 8101.3

Annotations:

Z
715.8 17715.3

Annotations:

^{0,4}A_{GalNAc}
732.6 5527.7
733.2 52796.3

Annotations:

Y
758.0 6652.0
768.2 4350.7
774.3 3733.3

Annotations:

YY
782.6 1025.7
798.4 1601.7
801.2 5919.7
804.2 840.3
810.1 2736.3
819.2 15208.7
828.2 1233.3
840.3 3382.7
841.1 4921.7
843.0 3585.3
854.2 4000.3
858.1 19756.7
858.7 1.0
860.5 6092.0
861.2 61913.7

Annotations:

Z
862.0 0.7
869.9 9875.0
870.6 4544.3
873.0 868.3
878.5 692.3
879.2 114526.3

Annotations:

Y
879.9 0.3
882.3 5940.0
896.2 2916.3
897.1 707.7
900.2 19389.0

Annotations:

ZZ ZZ ZZ ZZ
900.9 0.7
902.1 1046.0
903.2 1794.3
914.1 2213.0
918.1 2064.0

Annotations:

YZ ZY ZY YZ ZY ZY YZ YZ
927.2 11881.0
932.1 7745.3
936.7 1676.7

Annotations:

YY YY YY YY
944.2 636.7
950.0 3165.7
956.3 1568.3
960.3 2755.0
965.9 1675.0
974.0 6453.7
974.6 1149.0
975.8 790.0
986.0 3242.3
987.1 2183.7
1004.2 14756.7
1016.3 1925.0

Annotations:

^{1,5}A_{GalNAc}Z ^{1,5}A_{GalNAc}Z
1021.7 2693.3
1028.5 747.7
1042.7 1606.3
1045.8 2307.7
1046.4 12573.3
1061.2 1187.0
1064.1 17683.3

Annotations:

Z Z
1069.3 1337.0
1080.2 1770.0

Annotations:

YZ ZY ZY ZY YZ YZ
1082.2 16188.7

Annotations:

Y Y
1097.1 1205.3
1134.0 3557.7
1166.0 9543.7
1184.3 10390.3
1202.3 4353.0
1226.2 7274.3

Annotations:

Z Z Z
1244.2 15015.0

Annotations:

Y Y Y
1244.8 1.3

Annotations:

Y Y Y
1269.4 664.0
1274.3 550.7
1288.3 7371.3
1330.3 62643.0
1331.3 5447.7
1348.2 15907.3
1348.9 0.7
1373.0 2189.3
1418.0 2398.3

There are 2 similar spectra:

Id Structure Score

522

0.76

2910

0.72
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