Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.
GlyToucan Accession Number: G63550TC
| Peak | Intensity |
|---|---|
| 363.8 | 4858.7 |
|
Annotations: B |
|
| 366.9 | 4634.7 |
|
Annotations: ^{2,4}A_{GlcNAc} |
|
| 368.1 | 1314.0 |
| 390.7 | 1763.7 |
| 408.4 | 1534.7 |
| 409.0 | 44521.3 |
| 410.0 | 1591.0 |
| 423.8 | 5827.7 |
| 425.3 | 2166.7 |
| 450.9 | 5021.7 |
| 454.6 | 966.7 |
| 508.0 | 7958.3 |
|
Annotations: BZ |
|
| 509.1 | 1205.0 |
| 510.0 | 4982.7 |
|
Annotations: B |
|
| 510.8 | 1985.7 |
| 521.3 | 1102.3 |
| 525.9 | 9751.3 |
|
Annotations: BY |
|
| 528.0 | 1883.0 |
|
Annotations: C |
|
| 545.3 | 1461.3 |
| 558.8 | 744.7 |
| 568.9 | 13971.0 |
|
Annotations: ZY |
|
| 570.3 | 4151.0 |
| 584.4 | 541.0 |
| 587.2 | 5537.0 |
|
Annotations: YY |
|
| 588.2 | 402.3 |
| 594.1 | 611.3 |
| 596.3 | 1070.7 |
| 600.7 | 584.0 |
| 604.1 | 2268.3 |
| 631.1 | 952.0 |
| 647.3 | 3211.0 |
| 654.0 | 4554.3 |
|
Annotations: BZ |
|
| 655.3 | 718.3 |
| 655.9 | 963.3 |
| 665.2 | 1041.7 |
| 670.0 | 1293.0 |
| 672.0 | 6214.7 |
|
Annotations: BY |
|
| 688.0 | 2100.7 |
| 689.2 | 2467.7 |
| 690.2 | 2127.0 |
|
Annotations: CY |
|
| 693.6 | 6439.0 |
| 696.2 | 638.3 |
| 707.4 | 1054.3 |
| 708.4 | 2084.3 |
| 709.8 | 921.7 |
| 711.1 | 8587.0 |
|
Annotations: BZ |
|
| 712.1 | 4761.7 |
| 713.3 | 1368.7 |
|
Annotations: ZZ |
|
| 716.0 | 2363.7 |
| 730.2 | 2890.0 |
| 731.0 | 6768.7 |
|
Annotations: Z |
|
| 732.2 | 510.7 |
|
Annotations: ^{2,4}A_{GalNAc}Y |
|
| 745.2 | 2255.0 |
| 749.1 | 19612.0 |
|
Annotations: Y |
|
| 750.2 | 5241.0 |
| 754.3 | 2568.3 |
|
Annotations: ZZ |
|
| 755.3 | 1116.3 |
|
Annotations: ^{1,3}A_{GalNAc}Z |
|
| 770.2 | 769.7 |
| 772.2 | 4384.7 |
|
Annotations: ZY |
|
| 773.1 | 739.0 |
|
Annotations: ^{1,3}A_{GalNAc}Y |
|
| 776.2 | 1794.0 |
|
Annotations: ^{2,5}A_{GalNAc}Y |
|
| 784.2 | 873.7 |
| 787.3 | 3024.0 |
| 793.0 | 2407.3 |
| 801.7 | 2703.0 |
| 807.9 | 1131.7 |
| 826.1 | 3612.3 |
| 827.3 | 2309.0 |
| 831.2 | 1167.3 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 832.7 | 4758.7 |
| 833.5 | 546.7 |
|
Annotations: ^{2,5}A_{GalNAc}Y |
|
| 835.2 | 6543.3 |
| 836.4 | 589.3 |
| 850.1 | 622.0 |
| 851.4 | 529.0 |
| 852.9 | 5710.7 |
| 853.5 | 2112.7 |
| 854.3 | 290.0 |
| 856.2 | 3619.7 |
| 857.1 | 3025.7 |
|
Annotations: BZ |
|
| 858.1 | 4411.3 |
| 865.3 | 1713.7 |
| 874.2 | 19805.3 |
| 875.1 | 2257.3 |
|
Annotations: BY |
|
| 877.3 | 8024.7 |
|
Annotations: Z |
|
| 878.0 | 2180.7 |
| 886.3 | 2871.0 |
|
Annotations: ^{1,5}A_{GalNAc}Z |
|
| 887.1 | 513.0 |
| 892.0 | 4764.7 |
| 893.4 | 1884.0 |
|
Annotations: CY |
|
| 895.1 | 33728.7 |
|
Annotations: Y |
|
| 895.8 | 10463.7 |
|
Annotations: Y |
|
| 896.5 | 1.3 |
| 910.1 | 1276.0 |
| 911.3 | 280.3 |
| 916.4 | 392.0 |
|
Annotations: ZZ |
|
| 916.9 | 6171.3 |
|
Annotations: ^{2,4}A_{GalNAc}Z |
|
| 918.3 | 716.0 |
| 933.4 | 1564.3 |
|
Annotations: ^{2,4}A_{GalNAc}Z |
|
| 934.2 | 35372.0 |
|
Annotations: Z |
|
| 935.2 | 12421.0 |
|
Annotations: ^{2,4}A_{GalNAc}Y |
|
| 948.2 | 2655.7 |
| 952.3 | 479.0 |
|
Annotations: Y |
|
| 953.5 | 311.3 |
| 972.2 | 5529.7 |
| 976.2 | 3656.7 |
|
Annotations: ^{1,3}A_{GalNAc}Y |
|
| 990.1 | 4798.7 |
| 991.1 | 1427.0 |
| 995.2 | 3562.3 |
|
Annotations: ^{2,5}A_{GalNAc}Y |
|
| 996.0 | 693.0 |
| 997.2 | 1812.0 |
| 1005.8 | 310.3 |
| 1013.3 | 273.7 |
| 1020.1 | 15419.3 |
| 1021.3 | 2954.7 |
| 1032.1 | 1238.7 |
|
Annotations: ^{1,5}A_{GalNAc}Z |
|
| 1033.3 | 1790.0 |
| 1037.2 | 7776.3 |
|
Annotations: B |
|
| 1038.2 | 27156.7 |
| 1039.0 | 4056.7 |
| 1042.0 | 2954.0 |
| 1055.1 | 954.3 |
|
Annotations: C |
|
| 1056.0 | 7944.7 |
| 1061.2 | 1893.7 |
| 1062.1 | 4861.7 |
| 1080.1 | 31368.7 |
|
Annotations: Z |
|
| 1081.1 | 15572.3 |
| 1081.7 | 0.3 |
| 1092.3 | 795.7 |
| 1096.0 | 542.0 |
|
Annotations: Z |
|
| 1096.5 | 1334.7 |
|
Annotations: Z |
|
| 1097.2 | 813.0 |
|
Annotations: ^{2,4}A_{GalNAc} |
|
| 1098.1 | 10286.7 |
|
Annotations: Y |
|
| 1099.3 | 3272.7 |
| 1100.2 | 524.3 |
| 1102.0 | 1028.0 |
| 1110.1 | 3794.7 |
| 1115.0 | 1198.0 |
| 1116.5 | 825.3 |
| 1122.5 | 1219.3 |
| 1136.5 | 647.3 |
| 1141.9 | 3499.7 |
|
Annotations: ^{2,5}A_{GalNAc} |
|
| 1152.1 | 20479.3 |
| 1153.3 | 1270.0 |
| 1157.9 | 5701.0 |
|
Annotations: ^{0,2}A_{GalNAc} |
|
| 1159.3 | 8107.0 |
| 1167.5 | 527.7 |
| 1171.1 | 542.0 |
| 1176.2 | 3477.7 |
| 1177.1 | 1094.0 |
| 1194.5 | 1149.7 |
| 1200.2 | 53295.7 |
| 1201.2 | 32690.7 |
| 1216.1 | 884.7 |
| 1218.3 | 52442.0 |
| 1219.1 | 10079.3 |
| 1242.3 | 1091.3 |
| 1243.2 | 1414.0 |
| 1249.2 | 1264.7 |