Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.

PubMed Entry

GlyToucan Accession Number: G63550TC

Peak Intensity
363.8 4858.7

Annotations:

B
366.9 4634.7

Annotations:

^{2,4}A_{GlcNAc}
368.1 1314.0
390.7 1763.7
408.4 1534.7
409.0 44521.3
410.0 1591.0
423.8 5827.7
425.3 2166.7
450.9 5021.7
454.6 966.7
508.0 7958.3

Annotations:

BZ
509.1 1205.0
510.0 4982.7

Annotations:

B
510.8 1985.7
521.3 1102.3
525.9 9751.3

Annotations:

BY CZ
528.0 1883.0

Annotations:

C
545.3 1461.3
558.8 744.7
568.9 13971.0

Annotations:

ZY YZ YZ ZY
570.3 4151.0
584.4 541.0
587.2 5537.0

Annotations:

YY YY
588.2 402.3
594.1 611.3
596.3 1070.7
600.7 584.0
604.1 2268.3
631.1 952.0
647.3 3211.0
654.0 4554.3

Annotations:

BZ
655.3 718.3
655.9 963.3
665.2 1041.7
670.0 1293.0
672.0 6214.7

Annotations:

BY CZ
688.0 2100.7
689.2 2467.7
690.2 2127.0

Annotations:

CY
693.6 6439.0
696.2 638.3
707.4 1054.3
708.4 2084.3
709.8 921.7
711.1 8587.0

Annotations:

BZ
712.1 4761.7
713.3 1368.7

Annotations:

ZZ
716.0 2363.7
730.2 2890.0
731.0 6768.7

Annotations:

Z
732.2 510.7

Annotations:

^{2,4}A_{GalNAc}Y
745.2 2255.0
749.1 19612.0

Annotations:

Y
750.2 5241.0
754.3 2568.3

Annotations:

ZZ
755.3 1116.3

Annotations:

^{1,3}A_{GalNAc}Z
770.2 769.7
772.2 4384.7

Annotations:

ZY YZ
773.1 739.0

Annotations:

^{1,3}A_{GalNAc}Y
776.2 1794.0

Annotations:

^{2,5}A_{GalNAc}Y
784.2 873.7
787.3 3024.0
793.0 2407.3
801.7 2703.0
807.9 1131.7
826.1 3612.3
827.3 2309.0
831.2 1167.3

Annotations:

^{0,2}A_{GalNAc}Z
832.7 4758.7
833.5 546.7

Annotations:

^{2,5}A_{GalNAc}Y
835.2 6543.3
836.4 589.3
850.1 622.0
851.4 529.0
852.9 5710.7
853.5 2112.7
854.3 290.0
856.2 3619.7
857.1 3025.7

Annotations:

BZ
858.1 4411.3
865.3 1713.7
874.2 19805.3
875.1 2257.3

Annotations:

BY CZ
877.3 8024.7

Annotations:

Z
878.0 2180.7
886.3 2871.0

Annotations:

^{1,5}A_{GalNAc}Z
887.1 513.0
892.0 4764.7
893.4 1884.0

Annotations:

CY
895.1 33728.7

Annotations:

Y
895.8 10463.7

Annotations:

Y
896.5 1.3
910.1 1276.0
911.3 280.3
916.4 392.0

Annotations:

ZZ
916.9 6171.3

Annotations:

^{2,4}A_{GalNAc}Z
918.3 716.0
933.4 1564.3

Annotations:

^{2,4}A_{GalNAc}Z
934.2 35372.0

Annotations:

Z
935.2 12421.0

Annotations:

^{2,4}A_{GalNAc}Y
948.2 2655.7
952.3 479.0

Annotations:

Y
953.5 311.3
972.2 5529.7
976.2 3656.7

Annotations:

^{1,3}A_{GalNAc}Y
990.1 4798.7
991.1 1427.0
995.2 3562.3

Annotations:

^{2,5}A_{GalNAc}Y ^{0,2}A_{GalNAc}Y
996.0 693.0
997.2 1812.0
1005.8 310.3
1013.3 273.7
1020.1 15419.3
1021.3 2954.7
1032.1 1238.7

Annotations:

^{1,5}A_{GalNAc}Z
1033.3 1790.0
1037.2 7776.3

Annotations:

B
1038.2 27156.7
1039.0 4056.7
1042.0 2954.0
1055.1 954.3

Annotations:

C
1056.0 7944.7
1061.2 1893.7
1062.1 4861.7
1080.1 31368.7

Annotations:

Z
1081.1 15572.3
1081.7 0.3
1092.3 795.7
1096.0 542.0

Annotations:

Z
1096.5 1334.7

Annotations:

Z
1097.2 813.0

Annotations:

^{2,4}A_{GalNAc}
1098.1 10286.7

Annotations:

Y
1099.3 3272.7
1100.2 524.3
1102.0 1028.0
1110.1 3794.7
1115.0 1198.0
1116.5 825.3
1122.5 1219.3
1136.5 647.3
1141.9 3499.7

Annotations:

^{2,5}A_{GalNAc}
1152.1 20479.3
1153.3 1270.0
1157.9 5701.0

Annotations:

^{0,2}A_{GalNAc}
1159.3 8107.0
1167.5 527.7
1171.1 542.0
1176.2 3477.7
1177.1 1094.0
1194.5 1149.7
1200.2 53295.7
1201.2 32690.7
1216.1 884.7
1218.3 52442.0
1219.1 10079.3
1242.3 1091.3
1243.2 1414.0
1249.2 1264.7

There are 1 similar spectra:

Id Structure Score

3014

0.54
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