Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.
Peak | Intensity |
---|---|
366.6 | 12324.8 |
367.2 | 1515.8 |
Annotations: ^{2,4}A_{GlcNAc} ^{2,4}A_{GlcNAc} |
|
370.4 | 8075.0 |
381.1 | 29000.5 |
Annotations: ^{3,5}A_{GlcNAc} |
|
382.9 | 11580.0 |
389.0 | 101718.0 |
Annotations: ZZ ZZ |
|
390.2 | 6466.5 |
393.4 | 9918.8 |
405.9 | 9580.3 |
407.0 | 61878.0 |
Annotations: ZY YZ YZ ZY |
|
408.0 | 7056.3 |
Annotations: ^{1,3}A_{GlcNAc} |
|
408.9 | 176223.5 |
410.2 | 4787.0 |
442.0 | 11202.0 |
460.1 | 2266.5 |
465.4 | 13638.5 |
492.0 | 18715.3 |
501.8 | 7797.8 |
508.9 | 8624.8 |
510.1 | 69258.3 |
Annotations: B B |
|
511.1 | 5157.3 |
532.3 | 18088.8 |
543.7 | 7716.0 |
550.1 | 14376.5 |
551.0 | 35691.0 |
Annotations: ZZ ZZ |
|
568.9 | 50094.5 |
Annotations: ZY YZ YZ ZY |
|
570.0 | 129072.5 |
571.2 | 86848.0 |
574.0 | 4393.8 |
584.2 | 8077.3 |
587.1 | 18370.8 |
Annotations: YY YY |
|
592.2 | 59638.3 |
Annotations: ZZ |
|
593.2 | 7678.3 |
610.0 | 2997.8 |
Annotations: ZY YZ |
|
612.0 | 44631.0 |
621.0 | 1098.3 |
625.3 | 26067.3 |
625.9 | 0.8 |
628.9 | 5501.0 |
631.5 | 3195.0 |
649.0 | 4759.3 |
655.1 | 11217.8 |
656.0 | 575.5 |
667.0 | 20853.0 |
671.3 | 3078.5 |
673.1 | 206168.5 |
674.2 | 38686.0 |
685.3 | 960.8 |
691.2 | 94878.8 |
692.2 | 25840.3 |
694.3 | 26877.5 |
698.1 | 5901.8 |
701.4 | 7719.5 |
711.9 | 12152.5 |
715.2 | 873857.0 |
Annotations: Z Z |
|
716.1 | 294705.0 |
716.7 | 0.5 |
727.5 | 5017.3 |
731.2 | 14816.5 |
733.2 | 1150135.0 |
Annotations: Y Y |
|
734.2 | 286916.0 |
734.7 | 1.8 |
749.9 | 6774.3 |
754.1 | 2277.0 |
Annotations: ZZ ZZ |
|
755.1 | 4686.5 |
757.1 | 14534.0 |
768.2 | 2945.0 |
771.9 | 29942.0 |
Annotations: ZY YZ ZY YZ |
|
774.2 | 4581.5 |
779.8 | 3294.0 |
781.2 | 11403.8 |
782.3 | 5331.8 |
787.1 | 5283.3 |
789.9 | 3489.8 |
Annotations: YY YY |
|
792.2 | 4680.3 |
792.9 | 7457.0 |
798.1 | 3048.5 |
799.2 | 2557.0 |
800.2 | 11790.0 |
803.7 | 23328.8 |
805.2 | 22056.8 |
809.8 | 2839.0 |
810.9 | 3720.8 |
816.2 | 5840.5 |
828.1 | 79401.8 |
830.2 | 9855.8 |
839.8 | 15244.8 |
840.8 | 6330.3 |
858.1 | 66443.5 |
859.1 | 101879.5 |
859.8 | 7.5 |
861.4 | 3549.8 |
865.2 | 5821.8 |
870.3 | 15745.8 |
871.0 | 12063.0 |
872.0 | 13182.3 |
876.2 | 32873.3 |
876.8 | 9539.8 |
877.5 | 4.3 |
886.2 | 8082.5 |
887.5 | 12046.0 |
894.4 | 4494.8 |
896.7 | 2701.5 |
900.3 | 58217.0 |
901.1 | 49282.3 |
917.3 | 33833.0 |
918.1 | 481686.8 |
Annotations: Z Z |
|
919.2 | 143816.0 |
919.8 | 4.0 |
936.2 | 88450.3 |
Annotations: Y Y |
|
936.7 | 1.8 |
Annotations: Y Y |
|
937.4 | 17894.8 |
961.0 | 8231.3 |
965.4 | 6830.8 |
969.2 | 9952.3 |
982.1 | 3819.3 |
1006.1 | 5352.0 |
1017.3 | 3072.5 |
1038.1 | 33926.0 |
1039.1 | 3496.3 |
1045.4 | 7169.8 |
1057.4 | 3180.8 |
1080.4 | 74115.5 |
Annotations: Z Z |
|
1081.1 | 9042.0 |
1082.2 | 7063.0 |
1084.0 | 2786.8 |
1098.2 | 76578.8 |
Annotations: Y Y |
|
1099.3 | 46792.5 |
1125.2 | 2310.3 |
1135.1 | 7843.8 |
1142.2 | 20849.8 |
1142.9 | 0.3 |
1152.2 | 3353.8 |
1162.2 | 1818.5 |
1166.2 | 10184.3 |
1169.9 | 23158.8 |
1184.4 | 179145.8 |
1185.3 | 80851.8 |
1198.3 | 8123.3 |
1201.6 | 21558.0 |
1202.6 | 58746.3 |
1203.4 | 59384.8 |
1204.0 | 1.8 |
1208.6 | 17863.5 |
1260.6 | 2058.8 |
1284.0 | 1035.8 |
1317.5 | 1666.0 |