Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.
| Peak | Intensity |
|---|---|
| 366.6 | 12324.8 |
| 367.2 | 1515.8 |
|
Annotations: ^{2,4}A_{GlcNAc} |
|
| 370.4 | 8075.0 |
| 381.1 | 29000.5 |
|
Annotations: ^{3,5}A_{GlcNAc} |
|
| 382.9 | 11580.0 |
| 389.0 | 101718.0 |
|
Annotations: ZZ |
|
| 390.2 | 6466.5 |
| 393.4 | 9918.8 |
| 405.9 | 9580.3 |
| 407.0 | 61878.0 |
|
Annotations: ZY |
|
| 408.0 | 7056.3 |
|
Annotations: ^{1,3}A_{GlcNAc} |
|
| 408.9 | 176223.5 |
| 410.2 | 4787.0 |
| 442.0 | 11202.0 |
| 460.1 | 2266.5 |
| 465.4 | 13638.5 |
| 492.0 | 18715.3 |
| 501.8 | 7797.8 |
| 508.9 | 8624.8 |
| 510.1 | 69258.3 |
|
Annotations: B |
|
| 511.1 | 5157.3 |
| 532.3 | 18088.8 |
| 543.7 | 7716.0 |
| 550.1 | 14376.5 |
| 551.0 | 35691.0 |
|
Annotations: ZZ |
|
| 568.9 | 50094.5 |
|
Annotations: ZY |
|
| 570.0 | 129072.5 |
| 571.2 | 86848.0 |
| 574.0 | 4393.8 |
| 584.2 | 8077.3 |
| 587.1 | 18370.8 |
|
Annotations: YY |
|
| 592.2 | 59638.3 |
|
Annotations: ZZ |
|
| 593.2 | 7678.3 |
| 610.0 | 2997.8 |
|
Annotations: ZY |
|
| 612.0 | 44631.0 |
| 621.0 | 1098.3 |
| 625.3 | 26067.3 |
| 625.9 | 0.8 |
| 628.9 | 5501.0 |
| 631.5 | 3195.0 |
| 649.0 | 4759.3 |
| 655.1 | 11217.8 |
| 656.0 | 575.5 |
| 667.0 | 20853.0 |
| 671.3 | 3078.5 |
| 673.1 | 206168.5 |
| 674.2 | 38686.0 |
| 685.3 | 960.8 |
| 691.2 | 94878.8 |
| 692.2 | 25840.3 |
| 694.3 | 26877.5 |
| 698.1 | 5901.8 |
| 701.4 | 7719.5 |
| 711.9 | 12152.5 |
| 715.2 | 873857.0 |
|
Annotations: Z |
|
| 716.1 | 294705.0 |
| 716.7 | 0.5 |
| 727.5 | 5017.3 |
| 731.2 | 14816.5 |
| 733.2 | 1150135.0 |
|
Annotations: Y |
|
| 734.2 | 286916.0 |
| 734.7 | 1.8 |
| 749.9 | 6774.3 |
| 754.1 | 2277.0 |
|
Annotations: ZZ |
|
| 755.1 | 4686.5 |
| 757.1 | 14534.0 |
| 768.2 | 2945.0 |
| 771.9 | 29942.0 |
|
Annotations: ZY |
|
| 774.2 | 4581.5 |
| 779.8 | 3294.0 |
| 781.2 | 11403.8 |
| 782.3 | 5331.8 |
| 787.1 | 5283.3 |
| 789.9 | 3489.8 |
|
Annotations: YY |
|
| 792.2 | 4680.3 |
| 792.9 | 7457.0 |
| 798.1 | 3048.5 |
| 799.2 | 2557.0 |
| 800.2 | 11790.0 |
| 803.7 | 23328.8 |
| 805.2 | 22056.8 |
| 809.8 | 2839.0 |
| 810.9 | 3720.8 |
| 816.2 | 5840.5 |
| 828.1 | 79401.8 |
| 830.2 | 9855.8 |
| 839.8 | 15244.8 |
| 840.8 | 6330.3 |
| 858.1 | 66443.5 |
| 859.1 | 101879.5 |
| 859.8 | 7.5 |
| 861.4 | 3549.8 |
| 865.2 | 5821.8 |
| 870.3 | 15745.8 |
| 871.0 | 12063.0 |
| 872.0 | 13182.3 |
| 876.2 | 32873.3 |
| 876.8 | 9539.8 |
| 877.5 | 4.3 |
| 886.2 | 8082.5 |
| 887.5 | 12046.0 |
| 894.4 | 4494.8 |
| 896.7 | 2701.5 |
| 900.3 | 58217.0 |
| 901.1 | 49282.3 |
| 917.3 | 33833.0 |
| 918.1 | 481686.8 |
|
Annotations: Z |
|
| 919.2 | 143816.0 |
| 919.8 | 4.0 |
| 936.2 | 88450.3 |
|
Annotations: Y |
|
| 936.7 | 1.8 |
|
Annotations: Y |
|
| 937.4 | 17894.8 |
| 961.0 | 8231.3 |
| 965.4 | 6830.8 |
| 969.2 | 9952.3 |
| 982.1 | 3819.3 |
| 1006.1 | 5352.0 |
| 1017.3 | 3072.5 |
| 1038.1 | 33926.0 |
| 1039.1 | 3496.3 |
| 1045.4 | 7169.8 |
| 1057.4 | 3180.8 |
| 1080.4 | 74115.5 |
|
Annotations: Z |
|
| 1081.1 | 9042.0 |
| 1082.2 | 7063.0 |
| 1084.0 | 2786.8 |
| 1098.2 | 76578.8 |
|
Annotations: Y |
|
| 1099.3 | 46792.5 |
| 1125.2 | 2310.3 |
| 1135.1 | 7843.8 |
| 1142.2 | 20849.8 |
| 1142.9 | 0.3 |
| 1152.2 | 3353.8 |
| 1162.2 | 1818.5 |
| 1166.2 | 10184.3 |
| 1169.9 | 23158.8 |
| 1184.4 | 179145.8 |
| 1185.3 | 80851.8 |
| 1198.3 | 8123.3 |
| 1201.6 | 21558.0 |
| 1202.6 | 58746.3 |
| 1203.4 | 59384.8 |
| 1204.0 | 1.8 |
| 1208.6 | 17863.5 |
| 1260.6 | 2058.8 |
| 1284.0 | 1035.8 |
| 1317.5 | 1666.0 |