MIRAGE upload

Structural determination of neutral O-linked oligosaccharide alditols by negative ion LC-electrospray-MSn.

GlyToucan Accession Number: G04459VF

Peak	Intensity
340.1	322.6
340.8	1331.6
370.7	1577.6
383.7	2781.8
Annotations: YY
388.9	11238.4
389.5	813.0
455.1	986.0
456.2	408.4
Annotations: ^{0,3}X_{Fuc}Y ^{3,5}X_{Gal}Y ^{3,5}X_{GalNAc}
460.2	705.2
463.9	554.8
Annotations: ^{1,5}A_{GalNAc}Z
471.1	711.2
473.8	162.8
474.8	903.4
482.4	412.0
Annotations: ^{1,5}A_{GalNAc}Y
490.8	2707.8
492.0	855.4
Annotations: BZ BZ
494.2	320.8
509.2	5229.4
512.1	13498.4
Annotations: Z
513.3	7355.4
530.0	37023.6
Annotations: Y
531.2	3675.2
542.1	101.6
551.1	267.8
553.0	7588.4
Annotations: YZ ZY
570.0	374.8
Annotations: ^{0,4}A_{GalNAc}Y ^{0,4}A_{GalNAc}Y C^{0,2}X_{Fuc} C^{2,5}X_{Gal} C^{0,2}X_{Fuc}
571.0	223.4
Annotations: YY
583.4	1099.0
591.1	503.6
595.5	1444.4
606.8	439.4
614.0	970.6
Annotations: C^{1,3}X_{Fuc} C^{2,4}X_{Fuc} C^{0,4}X_{Gal} C^{2,4}X_{Gal} C^{1,3}X_{Fuc} C^{2,4}X_{Fuc} ^{1,3}X_{GalNAc}Z ^{1,3}X_{GalNAc}Z
619.7	927.6
621.0	6382.6
625.1	3582.2
Annotations: ^{1,4}X_{Gal}Z Z^{1,4}X_{Gal}
626.2	88.8
637.2	8886.4
637.8	231.0
638.9	524.6
654.2	2405.8
655.2	28982.0
Annotations: ^{1,3}X_{Gal}Z Z^{1,3}X_{Gal} ^{2,4}X_{GalNAc}Z ^{2,4}X_{GalNAc}Z
656.2	16451.0
Annotations: B
657.3	1071.4
663.6	228.0
666.9	3474.2
668.1	2028.0
670.1	1195.4
673.1	1831.4
Annotations: ^{1,3}X_{Gal}Y Y^{1,3}X_{Gal} ^{2,4}X_{GalNAc}Y ^{2,4}X_{GalNAc}Y
678.6	1135.0
679.3	6605.8
697.2	19140.0
Annotations: ZZ ZZ ZZ ZZ
698.1	5635.4
709.0	2982.4
715.0	2546.0
Annotations: YZ ZY YZ YZ YZ ZY ZY ZY
716.0	7844.8
Annotations: ^{0,4}A_{GalNAc}
734.1	278.2
801.0	8025.6
Annotations: ^{1,3}X_{Fuc}Z ^{2,4}X_{Fuc}Z ^{0,4}X_{Gal}Z ^{2,4}X_{Gal}Z Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc} Z^{0,4}X_{Gal} Z^{2,4}X_{Gal} Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc} ^{2,4}X_{Fuc}Z ^{1,3}X_{Fuc}Z
801.7	0.2
Annotations: ^{1,3}X_{Fuc}Z ^{2,4}X_{Fuc}Z ^{1,3}X_{Fuc}Z ^{2,4}X_{Fuc}Z ^{0,4}X_{Gal}Z ^{2,4}X_{Gal}Z Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc} Z^{0,4}X_{Gal} Z^{2,4}X_{Gal} Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc}
814.1	243.6
818.8	1401.6
819.4	16832.2
Annotations: ^{2,4}X_{GalNAc} ^{1,3}X_{Fuc}Y ^{2,4}X_{Fuc}Y ^{1,3}X_{Fuc}Y ^{2,4}X_{Fuc}Y ^{0,4}X_{Gal}Y ^{2,4}X_{Gal}Y Y^{1,3}X_{Fuc} Y^{2,4}X_{Fuc} Y^{0,4}X_{Gal} Y^{2,4}X_{Gal} Y^{1,3}X_{Fuc} Y^{2,4}X_{Fuc}
820.5	2235.2
836.0	209.0
839.9	625.8
844.2	965.0
852.6	586.8
861.1	51290.8
Annotations: Z Z
862.0	24135.0
862.8	0.2
873.2	449.4
875.2	1616.4
877.0	396.2
Annotations: YZ ZY ZY YZ YZ ZY
879.3	9368.8
Annotations: Y Y
880.3	5082.8
892.3	107.2
895.0	1847.4
Annotations: YY YY YY
898.6	185.2
903.3	1199.4
Annotations: ^{0,2}X_{Gal}Z Z^{0,2}X_{Gal} Z^{0,2}X_{Gal} ^{0,2}X_{Gal}Z ^{0,2}X_{Gal}Z ^{0,2}X_{Gal}Z
904.4	148.2
Annotations: ^{2,5}A_{GalNAc}Z ^{2,5}A_{GalNAc}Z ^{2,5}A_{GalNAc}Z
910.0	1364.4
912.3	3772.8
920.1	480.6
Annotations: ^{0,2}A_{GalNAc}Z ^{0,2}A_{GalNAc}Z ^{0,2}A_{GalNAc}Z
921.3	2505.4
Annotations: Y^{0,2}X_{Gal} ^{0,2}X_{Gal}Y ^{0,2}X_{Gal}Y Y^{0,2}X_{Gal} ^{0,2}X_{Gal}Y ^{0,2}X_{Gal}Y
929.2	1211.8
929.8	356.0
930.8	89.8
947.0	382.6
963.2	2024.2
Annotations: Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc} Z^{0,4}X_{Gal} Z^{2,4}X_{Gal} Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc} ^{0,4}X_{Gal}Z ^{0,4}X_{Gal}Z ^{2,4}X_{Gal}Z ^{2,4}X_{Gal}Z ^{0,4}X_{Gal}Z ^{2,4}X_{Gal}Z ^{0,4}X_{Gal}Z ^{2,4}X_{Gal}Z ^{1,3}X_{Fuc}Z ^{2,4}X_{Fuc}Z Z^{1,3}X_{Fuc} Z^{2,4}X_{Fuc} Z^{0,4}X_{Gal} Z^{2,4}X_{Gal} ^{1,3}X_{Fuc}Z ^{1,3}X_{Fuc}Z ^{2,4}X_{Fuc}Z ^{2,4}X_{Fuc}Z
967.6	2503.6
Annotations: ^{3,5}X_{Gal}Y ^{0,3}X_{Fuc}Y Y^{0,3}X_{Fuc} Y^{3,5}X_{Gal} ^{0,3}X_{Fuc}Y ^{0,3}X_{Fuc}Y Y^{0,3}X_{Fuc} Y^{3,5}X_{Gal} Y^{0,3}X_{Fuc} ^{3,5}X_{Gal}Y ^{3,5}X_{Gal}Y ^{3,5}X_{Gal}Y
977.4	167.0
981.8	171.8
Annotations: ^{0,4}X_{Gal}Y Y^{1,3}X_{Fuc} Y^{2,4}X_{Fuc} Y^{0,4}X_{Gal} Y^{2,4}X_{Gal} Y^{1,3}X_{Fuc} Y^{2,4}X_{Fuc} ^{0,4}X_{Gal}Y ^{0,4}X_{Gal}Y ^{2,4}X_{Gal}Y ^{2,4}X_{Gal}Y ^{1,3}X_{Gal} ^{2,4}X_{Gal}Y ^{0,4}X_{Gal}Y ^{1,3}X_{Gal} ^{2,4}X_{Gal}Y ^{1,3}X_{Fuc}Y ^{2,4}X_{Fuc}Y Y^{1,3}X_{Fuc} Y^{2,4}X_{Fuc} Y^{0,4}X_{Gal} Y^{2,4}X_{Gal} ^{1,3}X_{Fuc}Y ^{1,3}X_{Fuc}Y ^{2,4}X_{Fuc}Y ^{2,4}X_{Fuc}Y
984.4	319.6
995.6	212.6
1000.2	250.2
1000.9	815.8
1005.8	434.0
1023.3	18410.2
Annotations: Z Z Z
1024.1	5645.8
1025.2	3864.6
1028.4	739.4
1029.5	165.6
1031.2	330.2
1041.1	14757.2
Annotations: Y Y Y
1042.3	9192.4
1042.9	357.0
1048.0	763.0
1051.7	1211.8
1057.7	223.2
1062.0	297.0
1063.5	1001.2
1065.2	2944.2
1066.3	2600.2
1095.1	117.8
1103.0	191.6
1108.4	595.4
1110.4	170.4
1111.4	126.2
1113.3	93.4
Annotations: ^{0,3}X_{Fuc} ^{3,5}X_{Gal} ^{0,3}X_{Fuc} ^{3,5}X_{Gal} ^{0,3}X_{Fuc}
1115.3	1198.4
1125.3	999.2
1127.2	11314.4
Annotations: ^{1,3}X_{Fuc} ^{2,4}X_{Fuc} ^{0,4}X_{Gal} ^{2,4}X_{Gal} ^{1,3}X_{Fuc} ^{2,4}X_{Fuc} ^{0,4}X_{Gal} ^{2,4}X_{Gal} ^{1,3}X_{Fuc} ^{2,4}X_{Fuc}
1128.2	9669.6
1135.3	616.6
1143.6	792.0
Annotations: ^{0,4}X_{Fuc} ^{0,4}X_{Fuc} ^{0,4}X_{Fuc}
1144.5	313.8
1145.3	7370.8
1146.3	6820.2
1151.0	180.8
1156.0	240.8
1165.8	276.0
1169.3	453.2
1170.4	2278.4
1171.2	664.4
1209.4	524.4
1221.9	128.0
1223.0	1327.8
1224.2	266.8
1261.3	593.0