Efficient Chemoenzymatic Synthesis of an N-glycan Isomer Library
| Peak | Intensity |
|---|---|
| 186.14 | 13.7 |
|
Annotations: BZ |
|
| 202.88 | 24.9 |
| 204.08 | 3416.9 |
|
Annotations: B |
|
| 205.09 | 124.5 |
|
Annotations: ^{1,3}A_{Man}Z |
|
| 222.11 | 154.7 |
|
Annotations: C |
|
| 223.14 | 11.5 |
|
Annotations: ^{1,3}A_{Man}Y |
|
| 251.23 | 13.6 |
| 258.8 | 3.9 |
| 285.19 | 11.8 |
|
Annotations: YZ |
|
| 286.15 | 11.5 |
| 294.62 | 1.8 |
| 314.69 | 11.3 |
| 324.39 | 2.4 |
| 325.21 | 57.5 |
|
Annotations: BY |
|
| 326.2 | 15.2 |
| 343.27 | 13.1 |
|
Annotations: CY |
|
| 348.19 | 15.4 |
| 365.4 | 19.2 |
| 366.19 | 3066.3 |
|
Annotations: B |
|
| 367.2 | 262.2 |
|
Annotations: ^{0,4}A_{Man}Z |
|
| 367.81 | 6.7 |
|
Annotations: ^{2,5}A_{Man}Z |
|
| 375.72 | 9.6 |
|
Annotations: ^{0,2}A_{Man}Z |
|
| 384.25 | 3.4 |
|
Annotations: C |
|
| 385.35 | 1.2 |
|
Annotations: ^{0,2}A_{Man}Y |
|
| 387.12 | 18.7 |
| 393.16 | 3.5 |
| 394.98 | 13.7 |
| 395.91 | 76.3 |
| 398.74 | 9.3 |
|
Annotations: ^{3,5}A_{Man}Y |
|
| 400.23 | 10.8 |
| 407.29 | 47.2 |
|
Annotations: Z |
|
| 425.22 | 254.1 |
|
Annotations: Y |
|
| 426.34 | 11.5 |
|
Annotations: CZ |
|
| 438.87 | 6.7 |
| 447.21 | 164.3 |
|
Annotations: YZ |
|
| 447.85 | 12.2 |
| 450.24 | 9.2 |
| 456.29 | 8.6 |
|
Annotations: YY |
|
| 458.85 | 22.6 |
|
Annotations: ^{1,5}A_{Man} |
|
| 467.08 | 16.9 |
| 467.82 | 275.0 |
|
Annotations: Z |
|
| 468.43 | 20.2 |
| 475.79 | 74.2 |
| 476.83 | 819.2 |
|
Annotations: Y |
|
| 477.41 | 116.0 |
| 478.78 | 6.3 |
|
Annotations: ^{2,5}A_{Man} |
|
| 480.31 | 4.8 |
| 487.2 | 25.8 |
|
Annotations: B |
|
| 488.24 | 8.8 |
| 492.43 | 10.2 |
| 508.11 | 5.3 |
|
Annotations: B |
|
| 510.29 | 18.5 |
|
Annotations: BZ |
|
| 516.72 | 12.6 |
|
Annotations: C |
|
| 518.19 | 26.6 |
| 524.91 | 1.6 |
| 526.36 | 24.7 |
| 527.22 | 29.2 |
| 528.23 | 1813.6 |
|
Annotations: Z |
|
| 529.22 | 215.5 |
| 530.17 | 2.9 |
| 537.18 | 14.8 |
|
Annotations: Y |
|
| 540.04 | 50.9 |
|
Annotations: ZZ |
|
| 546.29 | 21.2 |
|
Annotations: CY |
|
| 547.79 | 14.4 |
| 548.88 | 788.0 |
|
Annotations: YZ |
|
| 549.94 | 14.6 |
| 551.33 | 11.2 |
|
Annotations: ZZ |
|
| 555.88 | 7.1 |
| 556.8 | 97.4 |
| 557.84 | 2126.6 |
|
Annotations: YY |
|
| 558.5 | 119.7 |
| 560.31 | 15.2 |
| 563.85 | 5.9 |
| 565.9 | 2.8 |
| 569.3 | 78.4 |
|
Annotations: YZ |
|
| 570.17 | 7.6 |
| 581.91 | 12.4 |
| 586.48 | 4.7 |
| 587.29 | 667.2 |
|
Annotations: YY |
|
| 588.28 | 99.8 |
| 589.11 | 10.5 |
| 591.08 | 12.0 |
| 593.86 | 32.7 |
| 600.19 | 17.1 |
| 601.28 | 1.3 |
| 608.21 | 11.9 |
| 609.35 | 45.8 |
|
Annotations: B |
|
| 611.43 | 13.4 |
| 617.89 | 1.8 |
|
Annotations: C |
|
| 620.83 | 27.2 |
| 628.78 | 85.8 |
| 629.89 | 659.5 |
|
Annotations: Z |
|
| 630.7 | 71.5 |
| 634.43 | 19.0 |
| 635.48 | 2.1 |
| 636.27 | 6.0 |
| 637.93 | 58.5 |
| 638.84 | 2661.8 |
|
Annotations: Y |
|
| 639.42 | 307.6 |
| 640.0 | 38.8 |
| 646.47 | 11.4 |
| 647.15 | 11.4 |
| 647.68 | 4.1 |
| 648.59 | 9.2 |
| 649.19 | 13.5 |
|
Annotations: BY |
|
| 649.9 | 20.9 |
| 653.24 | 6.7 |
| 659.38 | 7.5 |
| 662.78 | 8.2 |
| 668.88 | 14.4 |
| 672.37 | 5.8 |
| 674.85 | 15.2 |
| 685.12 | 6.6 |
| 688.15 | 25.3 |
| 689.54 | 23.6 |
| 690.29 | 2746.1 |
| 691.27 | 385.5 |
| 691.84 | 19.8 |
| 701.87 | 28.4 |
| 708.25 | 57.8 |
| 708.86 | 18.4 |
| 710.14 | 9.4 |
| 711.47 | 9.3 |
| 715.72 | 3.7 |
| 720.79 | 10.2 |
| 729.2 | 6.3 |
| 731.33 | 1048.7 |
|
Annotations: BY |
|
| 732.32 | 154.3 |
| 733.16 | 10.0 |
| 747.15 | 31.0 |
| 747.67 | 26.7 |
| 748.44 | 117.0 |
| 749.32 | 3739.4 |
|
Annotations: CY |
|
| 750.34 | 634.9 |
| 751.4 | 20.2 |
|
Annotations: ^{0,2}A_{Man}Z |
|
| 752.19 | 2.6 |
| 753.39 | 6.0 |
|
Annotations: ^{2,5}A_{Man}Y |
|
| 756.36 | 8.9 |
| 788.32 | 5.1 |
| 799.33 | 5.2 |
| 829.14 | 8.9 |
|
Annotations: CY |
|
| 829.96 | 6.0 |
| 834.1 | 4.2 |
|
Annotations: BZ |
|
| 850.39 | 63.2 |
| 851.47 | 76.5 |
| 852.37 | 4163.8 |
|
Annotations: BY |
|
| 853.37 | 932.3 |
| 854.43 | 13.0 |
| 855.16 | 19.2 |
| 857.39 | 4.0 |
| 870.38 | 30.2 |
|
Annotations: CY |
|
| 871.39 | 11.3 |
| 871.98 | 8.2 |
| 891.46 | 14.2 |
| 892.53 | 72.5 |
| 893.38 | 2409.5 |
|
Annotations: YZ |
|
| 894.38 | 440.3 |
| 894.95 | 9.7 |
| 895.59 | 18.0 |
| 907.48 | 12.2 |
| 909.66 | 207.1 |
| 910.57 | 135.3 |
| 911.36 | 10177.0 |
|
Annotations: YY |
|
| 912.39 | 2334.2 |
| 913.35 | 38.5 |
| 914.45 | 8.5 |
| 934.7 | 25.1 |
|
Annotations: Z |
|
| 935.48 | 16.1 |
| 952.41 | 50.3 |
|
Annotations: Y |
|
| 953.52 | 13.9 |
| 954.17 | 5.5 |
| 972.23 | 8.0 |
|
Annotations: ^{0,2}A_{Man} |
|
| 979.64 | 2.7 |
| 1012.13 | 11.4 |
| 1012.94 | 24.0 |
| 1013.51 | 30.0 |
| 1014.4 | 3620.8 |
|
Annotations: B |
|
| 1015.42 | 912.6 |
| 1016.37 | 54.8 |
| 1016.91 | 4.4 |
| 1032.37 | 26.2 |
|
Annotations: C |
|
| 1037.36 | 5.9 |
|
Annotations: BZ |
|
| 1038.14 | 7.9 |
| 1053.45 | 72.5 |
| 1054.45 | 77.2 |
| 1055.43 | 4728.4 |
|
Annotations: Z |
|
| 1056.43 | 1380.7 |
| 1057.38 | 49.1 |
| 1070.42 | 13.2 |
| 1071.64 | 339.3 |
| 1072.53 | 682.3 |
| 1073.39 | 18329.7 |
|
Annotations: Y |
|
| 1074.43 | 4961.3 |
| 1075.47 | 232.0 |
| 1077.98 | 1.4 |
|
Annotations: ZZ |
|
| 1114.53 | 38.0 |
|
Annotations: YY |
|
| 1200.19 | 17.7 |
| 1215.66 | 53.4 |
| 1216.71 | 53.3 |
| 1217.48 | 6850.9 |
|
Annotations: B |
|
| 1218.49 | 2413.6 |
| 1219.37 | 170.0 |
| 1222.27 | 16.9 |
| 1231.24 | 10.3 |
| 1232.58 | 13.9 |
| 1233.76 | 787.4 |
| 1234.65 | 949.6 |
| 1235.43 | 31032.9 |
|
Annotations: C |
|
| 1236.45 | 11818.5 |
| 1237.41 | 783.1 |
| 1238.32 | 30.7 |
| 1239.11 | 38.7 |
| 1242.54 | 5.6 |
| 1258.52 | 4.9 |
|
Annotations: Z |
|
| 1276.25 | 9.5 |
|
Annotations: Y |
|
There are not related spectra