MIRAGE upload

Structural diversity of human gastric mucin glycans

GlyToucan Accession Number: G74210VG

Peak	Intensity
245.9	1.1
264.14	0.9
282.03	161.6
Annotations: B
283.09	8.3
284.12	2.7
285.15	1.0
300.01	3.8
Annotations: C
342.2	3.6
Annotations: ^{0,4}A_{GalNAc}
365.42	1.0
371.98	6.9
386.23	1.5
387.07	3.6
404.8	1.8
407.19	15.5
Annotations: Z
408.13	2.3
425.15	2.1
Annotations: Y
427.23	6.7
428.08	5.2
428.51	0.7
435.23	0.8
444.04	0.8
445.17	21.5
446.16	2.2
451.09	0.8
457.24	1.0
463.05	1.1
464.1	0.9
465.29	1.1
469.19	3.8
469.82	0.9
470.27	0.8
472.13	0.8
485.89	0.8
487.14	85.7
Annotations: Z
488.16	14.2
505.17	1642.5
Annotations: Y
506.16	271.1
547.24	4.6
547.95	1.4
548.33	2.2
549.34	1.0
577.28	1.9
587.08	0.8
Annotations: Y
590.19	0.8
606.71	0.9
607.18	13.5
608.29	2.1
610.38	3.0
625.22	2.1
625.42	1.7
626.2	0.9
629.81	1.0
649.2	30.5
Annotations: Z
650.19	9.9
651.21	2.2
653.98	0.8
656.31	1.2
666.14	3.7
667.2	3949.5
Annotations: Y
668.2	847.8
669.22	1.9
672.08	1.2
680.36	1.5
693.41	1.0
694.4	3.0
695.02	0.8
698.88	1.0
709.8	0.8
710.22	1.3
711.25	1.0
717.06	0.8
720.86	1.3
723.37	0.8
726.26	0.9
727.69	0.8
733.97	1.9
738.08	0.9
738.99	1.2
746.11	1.5
750.33	2.0
750.88	1.0
751.1	1.1
753.26	25.5
754.32	5.8
758.53	0.9
767.06	1.3
767.26	1.3
768.95	1.2
769.32	1.7
770.36	1.5
771.16	10.1
771.48	1.6
772.37	3.3
773.23	1.2
775.81	2.5
776.36	1.4
776.92	1.5
777.3	2.5
781.96	2.6
783.33	1.7

There are 4 similar spectra:

Id	Structure	Score
338		1.00
156		0.99
3661		0.97
463		0.61

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass 812.25
(Calculated Monoisotopic)

Reducing End Reduced

Persubstitution Underivatised

Biological Context

Taxonomy - Homo Sapiens

Tissue - Stomach

HPLC

Column Custom made Hypercarb

Method

46 gradient with 10 run rate
10 mM Ammonium Bicarbonate
10 mM acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

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