MIRAGE upload

Structural diversity of human gastric mucin glycans

GlyToucan Accession Number: G02020YO

Peak	Intensity
203.8	1.8
Annotations: Z
204.19	1.7
Annotations: Z
205.19	2.1
219.94	52.6
Annotations: C
220.92	5.7
222.13	100.5
Annotations: Y
225.81	2.5
228.87	3.8
232.99	3.6
233.95	4.0
237.78	4.9
238.16	2.8
243.14	2.3
246.97	1386.8
248.01	57.6
249.36	2.6
250.12	2.9
258.09	3.7
270.86	1.9
272.41	1.8
288.18	4.6
288.97	3.1
Annotations: BZ
289.23	5.6
Annotations: BZ
298.15	3.2
299.14	1.7
299.55	1.9
300.14	8.3
301.09	3.2
305.47	3.1
306.89	368.2
Annotations: BY CZ
307.89	14.8
312.16	3.6
316.21	6.3
318.0	7.3
330.02	2.9
331.08	4.5
346.19	15.7
Annotations: BZ
347.15	5.7
348.2	17.2
Annotations: ZZ
349.1	3.4
377.21	2.0
406.16	2.3
407.22	7.5
408.13	27.6
409.17	2.8
422.09	3.2
425.33	3.3
426.84	8.0
451.88	2.7
452.17	5.1
470.27	11.7
471.35	2.3
483.36	2.7
494.31	4.7
495.12	2.4
497.27	2.6
509.24	4.7
510.18	363.9
Annotations: B
511.14	48.6
512.23	127.8
Annotations: Z
513.28	13.0
513.97	2.6
527.79	11.5
Annotations: C
528.23	5.0
Annotations: C
530.21	142.8
Annotations: Y
531.17	30.9
538.92	2.2
553.06	1.8
553.54	3.5
554.12	3.4
558.13	2.3
569.21	112.7
Annotations: Z
570.21	4.4
581.8	2.0
582.87	2.4
587.2	25.2
Annotations: Y
588.24	66.1
589.18	13.9
589.43	6.2
612.21	1.9
625.22	93.7
626.37	3.0
628.32	3.1
630.06	2.9
642.18	4.5
643.41	2.0
645.09	3.6
653.02	2.8
656.05	1.8
658.12	3.4
671.04	2.6
672.14	3.4
672.33	2.2
673.3	189.7
674.32	33.7
677.61	2.6
691.28	9.2
692.34	8.8
697.27	3.6
701.8	4.3
Annotations: B C Z Y B C Z Y B C Z Y

There are 3 similar spectra:

Id	Structure	Score
184		1.00
483		0.93
455		0.72

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass 732.30
(Calculated Monoisotopic)

Reducing End Reduced

Persubstitution Underivatised

Biological Context

Taxonomy - Homo Sapiens

Tissue - Stomach

HPLC

Column Custom made Hypercarb

Method

46 gradient with 10 run rate
10 mM Ammonium Bicarbonate
10 mM acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

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